Acetone sensor using lead foil as working electrode

被引:50
作者
Wang, Chia-Chi [1 ]
Weng, Yu-Ching [1 ]
Chou, Tse-Chuan [1 ]
机构
[1] Natl Cheng Kung Univ, Dept Chem Engn, Tainan 701, Taiwan
关键词
acetone; sensors; lead; amperometry reduction;
D O I
10.1016/j.snb.2006.07.003
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A new acetone sensor is developed by using a lead foil electrode in sodium tartrate solutions. The factors affecting the sensing characteristics, such as: applied potential, concentration of electrolyte, agitation rate and temperature were explored. The optimal operating conditions for the Pb foil electrode are 0.1 M sodium tartrate, 155 rpm agitation rate, 50 degrees C sensing temperature and applied potential in the range from -2.21 to -2.32 V (versus Ag/AgCl). The results reveal that the Pb foil electrode has a good linear relationship between response current and acetone concentration in the range from 50 to 250 ppm and this sensor has a fast response time of 18 s. (c) 2006 Elsevier B.V. All rights reserved.
引用
收藏
页码:591 / 595
页数:5
相关论文
共 15 条
  • [1] ANNO Y, 1995, SENSOR ACTUAT B-CHEM, V24, P623
  • [2] Application of principal component analysis for the characterisation of a piezoelectric sensors array
    Barkó, G
    Hlavay, J
    [J]. ANALYTICA CHIMICA ACTA, 1998, 367 (1-3) : 135 - 143
  • [3] Application of quadrupole mass spectrometer for the analysis of near-surface gas composition during DC sensor-tests
    Bene, R
    Kiss, G
    Perczel, IV
    Meyer, FA
    Reti, F
    [J]. VACUUM, 1998, 50 (3-4) : 331 - 337
  • [4] Determination of acetone in human breath by gas chromatography-mass spectrometry and solid-phase microextraction with on-fiber derivatization
    Deng, CH
    Zhang, J
    Yu, XF
    Zhang, W
    Zhang, XM
    [J]. JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2004, 810 (02): : 269 - 275
  • [5] Rapid determination of acetone in human plasma by gas chromatography-mass spectrometry and solid-phase microextraction with on-fiber derivatization
    Deng, CH
    Zhang, W
    Zhang, J
    Zhang, XM
    [J]. JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2004, 805 (02): : 235 - 240
  • [6] Cyclic voltammetry and passivation behaviour of lead in Na2HPO4 solution
    El-Naggar, MM
    [J]. JOURNAL OF POWER SOURCES, 2004, 126 (1-2) : 207 - 213
  • [7] Electrochemical behaviour of lead electrode in Na2SO4 solutions
    El-Sherbini, EF
    El Rehim, SSA
    [J]. MATERIALS CHEMISTRY AND PHYSICS, 2004, 88 (01) : 17 - 22
  • [8] Likhodii SS, 2002, CLIN CHEM, V48, P115
  • [9] LUND H, 1983, ORGANIC ELECTROCHEMI, P330
  • [10] Adsorption semiconductor sensor for diabetic ketoacidosis diagnosis
    Makisimovich, N
    Vorotyntsev, V
    Nikitina, N
    Kaskevich, O
    Karabun, P
    Martynenko, F
    [J]. SENSORS AND ACTUATORS B-CHEMICAL, 1996, 36 (1-3) : 419 - 421