1,3-Dithiol-2-ylium Compounds Derived from Substituted Butyrophenone

被引:0
作者
Sarbu, Laura Gabriela [1 ]
Apostu, Mircea Odin [1 ]
Sandu, Ioan Gabriel [2 ,3 ]
Manea, Liliana Rozemarie [4 ]
Bahrin, Lucian Gabriel [1 ]
机构
[1] Alexandru Ioan Cuza Univ, Dept Chem, Iasi 700506, Romania
[2] Gheorghe Asachi Tech Univ Iasi, Fac Mat Sci & Engn, Iasi 700050, Romania
[3] Romanian Inventors Forum, Iasi 700089, Romania
[4] Gheorghe Asachi Tech Univ, Fac Text Leather Engn & Ind Management, Iasi 700050, Romania
来源
REVISTA DE CHIMIE | 2014年 / 65卷 / 11期
关键词
butyrophenones; dithiocarbamates; 1,3-dithiolium salts; mesoionic compounds; X-ray crystallography; SELECTIVE SYNTHESIS; FLAVANONES;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A new class of 2-(dialkylamino)-1,3-dithiol-2-ylium compounds derived from substituted butyrophenone has been synthesized by the heterocondensation of the corresponding phenacyl carbodithioates. The title compounds have been obtained following a three step procedure that involves the reaction of 2-bromo-1-(2-hydrazyaryl)butan-1-one with various salts of dithiocarbamic acids, heterocydocondensation under acidic conditions and treatment with weak aqueous bases.
引用
收藏
页码:1327 / 1331
页数:5
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[1]   The antibacterial properties of sulfur containing flavonoids [J].
Bahrin, Lucian G. ;
Apostu, Mircea O. ;
Birsa, Lucian M. ;
Stefan, Marius .
BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2014, 24 (10) :2315-2318
[2]  
Bahrin LG, 2014, REV CHIM-BUCHAREST, V65, P199
[3]  
Belei D., 2009, Acta Chem. Ias, V17, P197
[4]  
Belei D, 2014, REV CHIM-BUCHAREST, V65, P80
[5]   A Direct Synthesis of Octahydropyrrolo[2,1,5-cd]indolizin-6-one Derivatives [J].
Belei, Dalila ;
Abuhaie, Cristina ;
Bicu, Elena ;
Jones, Peter G. ;
Hopf, Henning ;
Birsa, Lucian M. .
SYNLETT, 2012, (04) :545-548
[6]   A Selective Synthesis of Enamines versus Aziridines [J].
Belei, Dalila ;
Bicu, Elena ;
Jones, Peter G. ;
Birsa, M. Lucian .
JOURNAL OF HETEROCYCLIC CHEMISTRY, 2011, 48 (01) :129-134
[7]   A New Synthetic Methodology for the Pyrrolidine Ring [J].
Belei, Dalila ;
Bicu, Elena ;
Jones, Peter G. ;
Birsa, M. Lucian .
SYNLETT, 2010, (06) :931-933
[8]   Solvatochromism of mesoionic iodo(1,3-dithiol-2-ylium-4-yl) phenolates [J].
Birsa, Lucian M. ;
Asaftei, Luliean V. .
MONATSHEFTE FUR CHEMIE, 2008, 139 (12) :1433-1438
[9]  
Birsa LM, 2014, REV CHIM-BUCHAREST, V65, P174
[10]  
BIRSA M.L., 2000, AN STIINT U AL I CUZ, V8, P325