Crystal structure of tris((2-benzimidazolyl)methyl)amine-(4-hydroxy-cinnamato)-manganese(II) 4-hydroxycinnamate dimethylformamide solvate hydrate (1:0.5:3.3), [Mn{N(C8H7N2)3}C6H4(OH)(CH)2COO}] [C6H4(OH)(CH)2COO]•0.5(CH3)2NCHO•3.3H2O

被引：2
作者：
Wu, Hui-Lu [1 ]
Dong, Wen-Kui [1 ]
Wang, Xiao-Long [1 ]
机构：
[1] Lanzhou Jiaotong Univ, Sch Chem & Biol Engn, Lanzhou 730070, Peoples R China
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2007年 / 222卷 / 01期
关键词：
D O I：
10.1524/ncrs.2007.0013
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
C43.50H45.10MnN7.50O9.80, triclinic, P (1) over bar (no. 2), a = 11.936(1) angstrom, b = 14.435(2) angstrom, c = 14.752(2) angstrom alpha = 83.052(2)degrees, beta = 89.970(2)degrees, gamma = 66.287(2)degrees, V = 2306.7 angstrom(3) Z = 2, R-gt(F) = 0.057, wR(ref)(F-2) = 0.198, T = 293 K.
引用
收藏
页码：36 / 38
页数：3
相关论文
共 9 条
[1]  
Branden C-I, 1975, ENZYMES
[2]   Utility and synthetic uses of Mannich reaction: An efficient route for synthesis of thiadiazino-[1,3,5][3,2-a]benzimidazoles [J].
El-Wareth, A ;
Sarhan, AO ;
Abdel-Hafez, SH ;
El-Sherief, H ;
Aboel-Fadl, T .
SYNTHETIC COMMUNICATIONS, 2006, 36 (08) :987-996
[3]  
Sheldrick G.M., 1993, PROGRAM CRYSTAL STRU
[4]   Synthesis, crystal structure and cyclic voltammetry of a copper(II) complex with tripod ligand tris(2-benzimidazolylmethyl)amine [J].
Su, ZX ;
Wan, YQ ;
Wu, HL .
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2005, 35 (07) :553-558
[5]   Synthesis, crystal structure and properties of manganese(II) complexes with the tripod ligand tris(2-benzimidazylmethyl) amine and α,β-unsaturated carboxylates [J].
Wu, HL ;
Gao, YC .
JOURNAL OF COORDINATION CHEMISTRY, 2006, 59 (02) :137-146
[6]   Synthesis, crystal structure and characterization of zinc(II) complexes with the tripod ligand tris(2-benzimidazolylmethyl) amine and α,β-unsaturated carboxylates [J].
Wu, HL ;
Gao, YC .
TRANSITION METAL CHEMISTRY, 2004, 29 (02) :175-179
[7]   Aqua[tris(1H-benzimidazol-2-ylmethyl)amine]copper(II)bis(perchlorate)4-nitropyridine N-oxide monohydrate [J].
Wu, Hui-Lu ;
Dong, Wen-Kui ;
Chen, Ying .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 :M1708-M1710
[8]   Synthesis, crystal structure and superoxide dismutase activity of a five-co-ordinated manganese(II) complex [J].
Xiang, DF ;
Duan, CY ;
Tan, XS ;
Hang, QW ;
Tang, WX .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1998, (07) :1201-1204
[9]  
Zhou WH, 1999, CHIN J STRUCT CHEM, V18, P204
1