Metallic sample preparation for phase transformation analysis

被引：17

作者：

Paganotti, A. ^{[1
]}

Bessa, C. V. X. ^{[1
,2
]}

Silva, L. S. ^{[1
]}

Silva, R. A. G. ^{[1
]}

机构：

[1] Univ Fed Sao Paulo, Lab Mat & Mech Mfg, Diadema, Brazil

[2] Maua Inst Technol, Sao Caetano do Sul, Brazil

来源：

METHODSX | 2019年 / 6卷

基金：

巴西圣保罗研究基金会;

关键词：

Metals and alloys; Sample preparations; Heat treatment; AG; MICROSTRUCTURE; TRANSITIONS; ALLOY;

D O I：

10.1016/j.mex.2019.09.041

中图分类号：

O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];

学科分类号：

07 ; 0710 ; 09 ;

摘要：

Metallic materials characterization is a important part of phase transformation studies, and the sample preparation plays a crucial role in the measured properties. The methodologies available are not fully described and refer in its majority only to iron-based and aluminum-based alloys focusing in industrial analysis. In this paper the authors fully described the preparation methodology for metallic samples used by their research group. This method aims to attend different characterization techniques, producing samples of complex metallic systems from pure base materials by arc melting. The melting of metallic ingots from pure base materials was fully described. The correct sample cutting, sanding and polishing procedures were described. A full detailed procedure is described to prepare the samples for different analyses. (C) 2019 The Author(s). Published by Elsevier B.V.

引用

页码：2348 / 2366

页数：19

共 34 条

[1]

[Anonymous], 2013, TOXICOLOGICAL REV ME

[2] Effects of Gd addition on the thermal and microstructural behaviors of the as-cast Cu-9 % Al and Cu-9 % Al-10 % Mn alloys [J].

Brazolin, G. F. ;

Canbay, C. Aksu ;

Ozgen, S. ;

Oliveira, A. B. ;

Silva, R. A. G. .

APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING, 2016, 122 (10)

[3]

Echlin P., 2009, Handbook of sample preparation for scanning electron microscopy and x-ray microanalysis

[4] FUNDAMENTAL-ASPECTS OF ELECTROPOLISHING [J].

LANDOLT, D .

ELECTROCHIMICA ACTA, 1987, 32 (01) :1-11

[5] Effect of cooling rate on the microstructure and microhardness of the CuZrAgAl alloy [J].

Liu, Y. ;

Blandin, J. J. ;

Suery, M. ;

Kapelski, G. .

MATERIALS CHARACTERIZATION, 2012, 70 :8-13

[6]

Manasijevic D, 2017, METALL MATER ENG, V23, P255, DOI 10.30544/321

[7] TEM sample preparation and FIB-induced damage [J].

Mayer, Joachim ;

Giannuzzi, Lucille A. ;

Kamino, Takeo ;

Michael, Joseph .

MRS BULLETIN, 2007, 32 (05) :400-407

[8]

Mayer S. T., 1992, Patent No. [5096550, 5096550(A)]

[9] Kinetics of bainite precipitation in the Cu69.3Al18.8Mn10.3Ag1.6 alloy [J].

Motta, M. B. J. L. ;

Adorno, A. T. ;

Santos, C. M. A. ;

Silva, R. A. G. .

MATERIALS CHEMISTRY AND PHYSICS, 2017, 188 :125-130

[10] A MAJOR REVISION OF IRON METEORITE COOLING RATES - AN EXPERIMENTAL-STUDY OF THE GROWTH OF THE WIDMANSTATTEN PATTERN [J].

NARAYAN, C ;

GOLDSTEIN, JI .

GEOCHIMICA ET COSMOCHIMICA ACTA, 1985, 49 (02) :397-410

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