Dielectric and magnetic characterization of barium hexaferrite ceramics

被引:24
作者
Castro, W. S. [1 ,2 ]
Correa, R. R. [2 ]
Paulim Filho, P. I. [3 ]
Rivas Mercury, J. M. [1 ,4 ]
Cabral, A. A. [1 ,5 ]
机构
[1] Fed Inst Educ Sci & Technol Maranhao IFMA, Postgrad Program Mat Engn PPGEM, BR-65030005 Sao Luis, MA, Brazil
[2] Fed Inst Educ Sci & Technol Maranhao IFMA, Dept Electroelect DEE, BR-65030005 Sao Luis, MA, Brazil
[3] Fed Univ Sao Carlos UFSCar, Mat Engn Dept DEMA, Sao Carlos, SP, Brazil
[4] Fed Inst Educ Sci & Technol Maranhao IFMA, Dept Chem DAQ, BR-65030005 Sao Luis, MA, Brazil
[5] Fed Inst Educ Sci & Technol Maranhao IFMA, Dept Phys DEFIS, BR-65030005 Sao Luis, MA, Brazil
关键词
Magnetic properties; Dielectric properties; Barium hexaferrites; NANOPARTICLES; FERRITE;
D O I
10.1016/j.ceramint.2014.08.064
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Barium hexaferrite (BHF) was obtained by high energy ball milling using milling power of 4:1 and 10:1 and milling times of 1 h and 10 h, hereinafter referred to as BHF411, BliF4110, BHF101 and BHF1010, respectively. After sintering at 1200 degrees C, the products were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The magnetic and dielectric properties were examined using a permeameter (8.4 kOe) and an impedance analyzer (300 MHz-1.1 GHz), respectively. The properties of coercivity and magnetic saturation of the BHF41 samples increased with milling time, but decreased over time for BHF101. At low frequencies, both BHF41 samples showed a slight variation in relative permittivity (epsilon'), but this property remained almost constant at high frequencies. On the other hand, the initial permittivity of BHF101 samples varied significantly at low frequencies, but was almost constant at high frequencies. All the BHF samples showed a decreasing behavior of tan delta at the highest frequencies. (C) 2014 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:241 / 246
页数:6
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