N-(2-Chlorobenzoyl)benzenesulfonamide

被引：5
|
作者：
Gowda, B. Thimme [1 ]
Foro, Sabine [2 ]
Suchetan, P. A. [1 ]
Fuess, Hartmut [2 ]
机构：
[1] Mangalore Univ, Dept Chem, Mangalagangothri 574199, Karnataka, India
[2] Tech Univ Darmstadt, Inst Mat Sci, D-64287 Darmstadt, Germany
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词：
Data-to-parameter ratio = 15.4; Disorder in main residue; Mean σ(C-C) = 0.004 Å; R factor = 0.041; Single-crystal X-ray study; T = 299 K; WR factor = 0.113;
D O I：
10.1107/S1600536809055482
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The asymmetric unit of the title compound, C(13)H(10)ClNO(3)S, contains two independent molecules, the chlorophenyl ring of one of them being disordered over two orientations with occupancies of 0.836 (2) and 0.164 (2). In one of the independent molecules, the sulfonyl-bound phenyl ring and the chlorophenyl ring form dihedral angles of 87.3 (1) and 46.8 (1)degrees, respectively, with the -S-NH-C=O segment, while in the other molecule the corresponding angles are 76.0 (1) and 39.6 (1)degrees. In the crystal, molecules are linked into tetrameric units by N-H center dot center dot center dot O hydrogen bonds.
引用
收藏
页码：O326 / U2130
页数：12
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