One-dimensional SnF2 single crystals in the inner channels of single-wall carbon nanotubes: I. Preparation and basic characterization

被引：11

作者：

Zakalyukin, R. M. ^{[1
]}

Demyanets, L. N. ^{[1
]}

Kiselev, N. A. ^{[1
]}

Kumskov, A. S. ^{[1
]}

Kislov, M. B. ^{[2
]}

Krestinin, A. V. ^{[2
]}

Hutchison, J. L. ^{[3
,4
]}

机构：

[1] Russian Acad Sci, AV Shubnikov Crystallog Inst, Moscow 119333, Russia

[2] Russian Acad Sci, Inst Problems Chem Phys, Chernogolovka 142432, Moscow Oblast, Russia

[3] Univ Oxford, Dept Mat, Oxford OX1 3PH, England

[4] Univ Oxford, Dept Mat, Oxford, England

来源：

CRYSTALLOGRAPHY REPORTS | 2010年 / 55卷 / 03期

基金：

俄罗斯基础研究基金会;

关键词：

STANNOUS FLUORIDE; ENCAPSULATED C-60; CAPILLARITY; GROWTH; SWNTS;

D O I：

10.1134/S1063774510030223

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

One-dimensional (1D) SnF2 single crystals have been obtained by crystallization from melt in the inner channels of single-wall carbon nanotubes (SWCNTs). SWCNTs with an inner diameter of 1.02-1.4 nm, synthesized by electric-arc discharge and chemically purified, were used for incorporation. The synthesized 1D SnF2 single crystal-SWCNT composites are basically characterized by X-ray diffraction, energy-dispersive analysis, electron microscopy, and chemical analysis. The characteristic motifs of tin cation distribution in the SWCNT inner channel confirm the formation of SnF2 single crystals.

引用

页码：507 / 512

页数：6

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