Plasma in-liquid method for reduction of zinc oxide in zinc nanoparticle synthesis

被引：8

作者：

Amaliyah, Novriany ^{[1
,2
]}

Mukasa, Shinobu ^{[1
]}

Nomura, Shinfuku ^{[1
]}

Toyota, Hiromichi ^{[1
]}

Kitamae, Tomohide ^{[1
]}

机构：

[1] Ehime Univ, Grad Sch Sci & Engn, Matsuyama, Ehime 7908577, Japan

[2] Hasanuddin Univ, Dept Mech Engn, Makassar 90245, Indonesia

来源：

MATERIALS RESEARCH EXPRESS | 2015年 / 2卷 / 02期

关键词：

MICROWAVE PLASMA; LASER-ABLATION; LARGE-SCALE; AIR; NANORODS;

D O I：

10.1088/2053-1591/2/2/025004

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Metal air-batteries with high-energy density are expected to be increasingly applied in electric vehicles. This will require a method of recycling air batteries, and reduction of metal oxide by generating plasma in liquid has been proposed as a possible method. Microwave-induced plasma is generated in ethanol as a reducing agent in which zinc oxide is dispersed. Analysis by energy-dispersive x-ray spectrometry (EDS) and x-ray diffraction (XRD) reveals the reduction of zinc oxide. According to images by transmission electron microscopy (TEM), cubic and hexagonal metallic zinc particles are formed in sizes of 30 to 200 nm. Additionally, spherical fiber flocculates approximately 180 nm in diameter are present.

引用

页数：9

共 34 条

[1]

Bergman M, 2013, THESIS CHALMERS U TE

[2] Materials science aspects of zinc-air batteries: A review [J].

Caramia V. ;

Bozzini B. .

Materials for Renewable and Sustainable Energy, 2014, 3 (02)

[3]

Ebrahim HA, 2001, CHEM ENG RES DES, V79, P62

[4] PbTiO3- and Pb(Zr,Ti)O3-Covered ZnO Nanorods [J].

Fujisawa, Hironori ;

Kuri, Ryohei ;

Shimizu, Masaru ;

Kotaka, Yasutoshi ;

Honda, Koichiro .

APPLIED PHYSICS EXPRESS, 2009, 2 (05)

[5] ZnO Nanobox Luminescent Source Fabricated by Three-Dimensional Nanotemplate Pulsed-Laser Deposition [J].

Hattori, Azusa N. ;

Ichimiya, Masayoshi ;

Ashida, Masaaki ;

Tanaka, Hidekazu .

APPLIED PHYSICS EXPRESS, 2012, 5 (12)

[6] Synthesis of tungsten trioxide nanoparticles by microwave plasma in liquid and analysis of physical properties [J].

Hattori, Yoshiaki ;

Nomura, Shinfuku ;

Mukasa, Shinobu ;

Toyota, Hiromichi ;

Inoue, Toru ;

Kasahara, Toshihiro .

JOURNAL OF ALLOYS AND COMPOUNDS, 2013, 560 :105-110

[7] Continuous synthesis of magnesium-hydroxide, zinc-oxide, and silver nanoparticles by microwave plasma in water [J].

Hattori, Yoshiaki ;

Mukasa, Shinobu ;

Toyota, Hiromichi ;

Inoue, Toru ;

Nomura, Shinfuku .

MATERIALS CHEMISTRY AND PHYSICS, 2011, 131 (1-2) :425-430

[8] Synthesis of zinc and zinc oxide nanoparticles from zinc electrode using plasma in liquid [J].

Hattori, Yoshiaki ;

Mukasa, Shinobu ;

Toyota, Hiromichi ;

Inoue, Toru ;

Nomura, Shinfuku .

MATERIALS LETTERS, 2011, 65 (02) :188-190

[9]

Int. Zinc Association, 2011, CLOS THE LOOP

[10] Synthesis of ZnO nanorods by nanoparticle assisted pulsed-laser deposition [J].

Kawakami, M ;

Hartanto, AB ;

Nakata, Y ;

Okada, T .

JAPANESE JOURNAL OF APPLIED PHYSICS PART 2-LETTERS, 2003, 42 (1A-B) :L33-L35

← 1 2 3 4 →