4-(3-Methoxyphenyl)-2,6-dimethylcyclohex-3-enecarboxylic acid

被引:3
作者
Xie, Songwen [1 ]
Nusbaum, Dannette A. [1 ]
Stein, Holly J. [1 ]
Pink, Maren [2 ]
机构
[1] Indiana Univ, Dept Nat Informat & Math Sci, Kokomo, IN 46904 USA
[2] Indiana Univ, Ctr Mol Struct, Bloomington, IN 47405 USA
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
基金
美国国家科学基金会;
关键词
D O I
10.1107/S1600536810018544
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The racemic title compound, C(16)H(20)O(3), was synthesized to study the hydrogen-bonding interaction of the two enantiomers in the solid state. In the crystal structure, R and S pairs of the racemate are linked by pairs of intermolecular O-H center dot center dot center dot O hydrogen bonds, producing centrosymmetric R(2)(2)(8) rings.
引用
收藏
页码:O1443 / U1709
页数:10
相关论文
共 11 条
  • [1] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS
    BERNSTEIN, J
    DAVIS, RE
    SHIMONI, L
    CHANG, NL
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) : 1555 - 1573
  • [2] AN EMPIRICAL CORRECTION FOR ABSORPTION ANISOTROPY
    BLESSING, RH
    [J]. ACTA CRYSTALLOGRAPHICA SECTION A, 1995, 51 : 33 - 38
  • [3] Bruker, 2007, APEX2 SAINT SADABS
  • [4] SIR2004:: an improved tool for crystal structure determination and refinement
    Burla, MC
    Caliandro, R
    Camalli, M
    Carrozzini, B
    Cascarano, GL
    De Caro, L
    Giacovazzo, C
    Polidori, G
    Spagna, R
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2005, 38 : 381 - 388
  • [5] A short history of SHELX
    Sheldrick, George M.
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
  • [6] 2,6-dimethyl-4-m-tolylcyclohex-3-enecarboxylic acid
    Xie, Songwen
    Stein, Holly J.
    Pink, Maren
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1869 - U3277
  • [7] Racemic 4-(4-tert-butylphenyl)-2,6-dimethylcyclohex-3-enecarboxylic acid
    Xie, Songwen
    O'Hearn, Caryn R.
    Robinson, Paul D.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O554 - U803
  • [8] Racemic 5-ethyl-2,6-dimethyl-4-p-tolyl-3-cyclohexenecarboxylic acid: an RS dimer
    Xie, Songwen
    Kenny, Colin
    Robinson, Paul D.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O3897 - U3826
  • [9] 2,6-Dimethyl-4-oxocyclohexanecarboxylic acid:: a meso keto acid
    Xie, Songwen
    Kenny, Colin
    Robinson, Paul D.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O1660 - O1662
  • [10] N,N′-Dicyclohexyl-N-[(1RS,2RS,6SR)-4-(4-methoxyphenyl)-2,6-dimethyl-3-cyclohexene-1-carbonyl]urea:: an unusual crystalline enantiomeric pairing
    Xie, SW
    Meyers, CY
    Robinson, PD
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2004, 60 : O1362 - O1364