In this study, we analyzed a tooth sample of a renal patient using wavelength-dispersive X-ray fluorescence (WDXRF) spectrometry and Fourier transform infrared (FT-IR) spectrometry to quantify major and trace elements, and heavy and toxic elements in particular. The elements detected and quantified in the tooth sample were calcium (Ca), phosphorus (P), carbon (C), oxygen (O), magnesium (Mg), sodium (Na), chlorine (CI), sulfur (S), potassium (K), silicon (Si), iron (Fe), aluminum (Al), zinc (Zn), strontium (Sr), chromium (Cr), nickel (Ni), copper (Cu), and zirconium (Zr). FT-IR spectrometry has been used to extract relevant information about the molecular contents of the tooth sample. We have compared our results with those obtained in the laboratory for the healthy subjects, and also with the values reported in the literature as obtained using XRF spectrometry only. Elements found in the tooth sample were correlated with the chronic kidney disease (CKD) of the patients. An outline of the XRF apparatus and applications of XRF as a tool for analyzing to dental specimens are also briefly highlighted.