Oscillatory pressure sintering: A new method for preparing WC-Co cemented carbides

被引:42
|
作者
Zhu, Tianbin [1 ,2 ]
Zhang, Jie [1 ,2 ]
An, Di [3 ]
Xie, Zhipeng [3 ]
Li, Yawei [1 ,2 ]
Sang, Shaobai [1 ,2 ]
Dai, Jinning [4 ]
机构
[1] Wuhan Univ Sci & Technol, State Key Lab Refractories & Met, Wuhan 430081, Hubei, Peoples R China
[2] Wuhan Univ Sci & Technol, Natl Provincial Joint Engn Res Ctr High Temp Mat, Wuhan 430081, Hubei, Peoples R China
[3] Tsinghua Univ, Sch Mat Sci & Engn, State Key Lab New Ceram & Fine Proc, Beijing 100084, Peoples R China
[4] Zhuzhou Wanrong New Mat Technol Co Ltd, Zhuzhou 412000, Peoples R China
基金
中国国家自然科学基金; 中国博士后科学基金;
关键词
Oscillatory pressure sintering (OPS); WC-Co cemented carbides; Microstructure; Mechanical properties; MECHANICAL-PROPERTIES; COMPOSITE POWDERS; MICROSTRUCTURE; TOUGHNESS; FRACTURE; VC; DENSIFICATION; STRENGTH; HARDNESS; COBALT;
D O I
10.1016/j.jallcom.2019.152521
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
WC-10 wt% Co cemented carbides were prepared by a new oscillatory pressure sintering (OPS) process in the present work, and the influence of sintering temperature on their microstructure and mechanical properties was mainly investigated. The results were also compared to the sample prepared via conventional hot pressing (HP) under a similar consolidation condition. The optimum OPS temperature was similar to 1310 degrees C; the denser sample with uniform microstructure could be obtained; the sample exhibited the highest flexural strength of 2431 MPa, Vickers hardness of 21.1 GPa and fracture toughness of 11.42 MPa m(1/2). Moreover, the OPS-fabricated sample displayed much better mechanical properties than that of HP-fabricated sample, which might greatly be related to the improved grain boundary sliding, plastic deformation and mass diffusion during the OPS process. This work demonstrates a new approach to prepare high-performance cemented carbides. (C) 2019 Elsevier B.V. All rights reserved.
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页数:5
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