Synthesis of 2,4,6-trinitro-2,4,6-triazacyclohexanone

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作者
Xi, MH [1 ]
Yao, QZ [1 ]
机构
[1] Nanjing Univ Sci & Technol, Nanjing 210094, Peoples R China
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O414.1 [热力学];
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摘要
The preparation of 2,4,6-trinitro-2,4,6-triazacyclohexanone is made by the acid-hydrolysis, nitration and condensation of hexame (HA) and urea seperately in the polyphosphoric acid-nitric acid and nitric acidsulphur ic acid mixtures. The yield of it's monomolecular products is over 98% which is maximum in all the present methods, The simple and convenient operation, and rich in raw mater ials are also the advantages of the method.
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页码:180 / 184
页数:5
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