Raman spectroscopic study of corroded historical glass

被引：1

作者：

Hruska, Branislav ^{[1
]}

Nowicka, Aleksandra ^{[1
]}

Chromcikova, Maria ^{[2
,3
]}

Greiner-Wrona, Elzbieta ^{[4
]}

Smolik, Jan ^{[5
]}

Soltezs, Vojtech ^{[6
]}

Liska, Marek ^{[2
,3
]}

机构：

[1] Alexander Dubcek Univ Trencin, FunGlass, Trencin, Slovakia

[2] FChPT STU, TnUAD, VILA Joined Glass Ctr IIC SAS, Trencin, Slovakia

[3] Slovak Acad Sci, Inst Inorgan Chem, Bratislava, Slovakia

[4] AGH Tech Univ Sci & Technol, Krakow, Poland

[5] Univ Pardubice, Fac Chem Technol, Dept Phys Chem, Pardubice, Czech Republic

[6] VUEZ As, Levice, Slovakia

来源：

INTERNATIONAL JOURNAL OF APPLIED GLASS SCIENCE | 2021年 / 12卷 / 04期

关键词：

glass corrosion; MCR; PCA; Raman spectroscopy;

D O I：

10.1111/ijag.16010

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

The corroded surfaces of historical glass samples were studied by micro-Raman spectroscopy. The spectra acquired from lateral and stratified mapping were analyzed by principal component analysis providing the number of linearly independent spectral components and by multivariate curve analysis resulting in spectrum of native glass and spectra of different corrosion products (loadings) and their relative abundances (scores) in each measured spot. The obtained results were qualified by comparison of results obtained by stratified mapping with the results of lateral mapping. On the basis of dominant scores, the lateral distribution of various corrosion products was identified. The quality of corrosion products was only roughly identified by the spectral database (S.T. Japan spectral database).

引用

页码：613 / 620

页数：8

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