One-pot synthesis of nanostructured CdS, CuS, and SnS by pulsed laser ablation in liquid environment and their antimicrobial activity

被引:97
作者
Mostafa, Ayman M. [1 ,2 ]
Mwafy, Eman A. [3 ]
Hasanin, Mohamed S. [4 ]
机构
[1] Natl Res Ctr, Laser Technol Unit, Ctr Excellent Adv Sci, 33 El Bohouth St,PO 12622, Giza, Egypt
[2] Natl Res Ctr, Dept Spect, Div Phys, 33 El Bohouth St,PO 12622, Giza, Egypt
[3] Natl Res Ctr, Dept Phys Chem, Inorgan Chem Ind & Mineral Resources Div, 33 El Bohouth St,PO 12622, Giza, Egypt
[4] Natl Res Ctr, Cellulose & Paper Dept, 33 El Bohouth St,PO 12622, Giza, Egypt
关键词
Laser ablation; Nanostructure; Antimicrobial; Metal sulfides; PLAL; CADMIUM-OXIDE NANOPARTICLES; CARBOXYMETHYL CELLULOSE; OPTICAL-PROPERTIES; SULFIDE; NANOCRYSTALS; MEDIA;
D O I
10.1016/j.optlastec.2019.105824
中图分类号
O43 [光学];
学科分类号
070207 ; 0803 ;
摘要
We describe here a generic method for producing high-quality metal sulfide nanoparticles of a controllable and narrow size distribution in the nano-metric range. Metal sulfide nanostructures (CdS, CuS, and SnS) are synthesized by using nanosecond pulsed laser ablation in a liquid solution containing sulfur precursor in just one step (one-pot versatile synthesis method). The optical properties have been studied using UV Visible spectroscopy showing the main characteristic transition peaks of metal sulfides. Transmission electron microscope (TEM) shows a uniform Smaller-sized and nearly spherical nanocrystals exhibited a cross lattice pattern. The structure study by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDX) reveal the purity and the spherical crystalline structure of all the prepared nano metal sulfides. After that, the antibacterial activity has been examined against four types of bacteria and unicellular fungi by using agar plate diffusion methods followed by studying the required time for killing. The tested microorganisms strain is showing that CuS nano particles have the highest antimicrobial activity.
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页数:6
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