Impact of Sandblasting on Morphology, Structure and Conductivity of Zirconia Dental Ceramics Material

被引:20
作者
Jakovac, Marko [1 ]
Klaser, Teodoro [2 ]
Radatovic, Borna [3 ]
Bafti, Arijeta [4 ]
Skoko, Zeljko [2 ]
Pavic, Luka [5 ]
Zic, Mark [5 ]
机构
[1] Univ Zagreb, Sch Dent Med, Dept Prosthodont, Gunduliceva 5, Zagreb 10000, Croatia
[2] Univ Zagreb, Fac Sci, Dept Phys, Bijenicka C 32, Zagreb 10000, Croatia
[3] Inst Phys, Ctr Excellence Adv Mat & Sensing Devices, Zagreb 10000, Croatia
[4] Univ Zagreb, Fac Chem Engn & Technol, Marulicev Trg 19, Zagreb 10000, Croatia
[5] Rudjer Boskovic Inst, POB 180, Zagreb 10000, Croatia
关键词
zirconia; sandblasting; PXRD; impedance; equivalent electrical circuit (EEC); conductivity; dental material; YTTRIA-STABILIZED ZIRCONIA; SHEAR BOND STRENGTH; FLEXURAL STRENGTH; RESIN CEMENT; IONIC-CONDUCTIVITY; SURFACE; LASER; GLASS; MICROSTRUCTURE; RESTORATIONS;
D O I
10.3390/ma14112834
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Over the last decade, zirconia (ZrO2)-based ceramic materials have become more applicable to modern dental medicine due to the sustained development of diverse computer-aided design/computer-aided manufacturing (CAD/CAM) systems. However, before the cementation and clinical application, the freshly prepared zirconia material (e.g., crowns) has to be processed by sandblasting in the dental laboratory. In this work, the impact of the sandblasting on the zirconia is monitored as changes in morphology (i.e., grains and cracks), and the presence of impurities might result in a poor adhesive bonding with cement. The sandblasting is conducted by using Al2O3 powder (25, 50, 110 and 125 mu m) under various amounts of air-abrasion pressure (0.1, 0.2, 0.4 and 0.6 MPa). There has been much interest in both the determination of the impact of the sandblasting on the zirconia phase transformations and conductivity. Morphology changes are observed by using Scanning Electron Microscope (SEM), the conductivity is measured by Impedance Spectroscopy (IS), and the phase transformation is observed by using Powder X-Ray Diffraction (PXRD). The results imply that even the application of the lowest amount of air-abrasion pressure and the smallest Al2O3 powder size yields a morphology change, a phase transformation and a material contamination.
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页数:12
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