Chiral Separation of Aspartic Acid by Thin-Layer Chromatography

被引:0
作者
Katiyar, Prashant K. [1 ]
Wala, Ravi Kabra [1 ]
机构
[1] Kanpur Inst Technol & Pharm, UPSIDC Ind Area, Kanpur 208001, Uttar Pradesh, India
关键词
Chiral separation; Aspartic acid; Arginine; Thin-layer chromatography; CAPILLARY ELECTROCHROMATOGRAPHY; AMINO-ACIDS; HPLC; SPECTROMETRY;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In this study, chiral separation of D/L-aspartic acid was achieved by thin layer chromatography using L-arginine as a chiral separator using the mobile phase as butanol:glacial acetic acid:water (70:10:20) and the visualizing agent is ninhydrin and butanol (20:10).
引用
收藏
页码:4945 / 4946
页数:2
相关论文
共 10 条
[1]   HPLC method for analysis of free amino acids in fish using o-phthaldialdehyde precolumn derivatization [J].
Antoine, FR ;
Wei, CI ;
Littell, RC ;
Marshall, MR .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1999, 47 (12) :5100-5107
[2]   Electrospray ionization nigh-resolution ion mobility spectrometry for the detection of organic compounds, 1. Amino acids [J].
Beegle, LW ;
Kanik, I ;
Matz, L ;
Hill, HH .
ANALYTICAL CHEMISTRY, 2001, 73 (13) :3028-3034
[3]   A new application of stopped-flow chiral HPLC: inversion of enantiomer elution order [J].
Cirilli, R ;
Ferretti, R ;
Gallinella, B ;
Zanitti, L ;
La Torre, F .
JOURNAL OF CHROMATOGRAPHY A, 2004, 1061 (01) :27-34
[5]   GAS CHROMATOGRAPHIC-MASS SPECTROMETRIC ANALYSIS OF OPTICALLY-ACTIVE METABOLITES AND DRUGS ON A NOVEL CHIRAL STATIONARY PHASE [J].
FRANK, H ;
NICHOLSON, GJ ;
BAYER, E .
JOURNAL OF CHROMATOGRAPHY, 1978, 146 (02) :197-206
[6]  
Gil-Av E, 1966, TETRAHEDRON LETT, V10, P1009
[7]   Applications of enantiomeric gas chromatography: A review [J].
He, LF ;
Beesley, TE .
JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, 2005, 28 (7-8) :1075-1114
[8]   Separation of enantiomers by capillary electrochromatography [J].
Lämmerhofer, M ;
Svec, F ;
Fréchet, JMJ ;
Lindner, W .
TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 2000, 19 (11) :676-698
[9]   Monolithic enantiomer-selective stationary phases for capillary electrochromatography [J].
Qin, Feng ;
Xie, Chuanhui ;
Yu, Zhiyuan ;
Kong, Liang ;
Ye, Mingliang ;
Zou, Hanfa .
JOURNAL OF SEPARATION SCIENCE, 2006, 29 (10) :1332-1343
[10]   Amino acid analysis by capillary electrophoresis electrospray ionization mass spectrometry [J].
Soga, T ;
Heiger, DN .
ANALYTICAL CHEMISTRY, 2000, 72 (06) :1236-1241