Preparation of two flavonoid glycosides with unique structures from barley seedlings by membrane separation technology and preparative high-performance liquid chromatography

被引：15

作者：

Chen, Tao ^{[1
]}

Li, Hong-mei ^{[1
,2
]}

Zou, Deng-Lang ^{[1
,2
]}

Du, Yu-Zhi ^{[1
]}

Shen, Yu-Hu ^{[1
]}

Li, Yulin ^{[1
]}

机构：

[1] Chinese Acad Sci, Northwest Inst Plateau Biol, Key Lab Tibetan Med Res, Xining 810001, Peoples R China

[2] Univ Chinese Acad Sci, Beijing, Peoples R China

来源：

JOURNAL OF SEPARATION SCIENCE | 2014年 / 37卷 / 24期

基金：

中国科学院西部之光基金;

关键词：

Barley seedlings; Lutonarin; Membrane separation technology; Response surface methodology; Saponarin; PURIFICATION; ACIDS;

D O I：

10.1002/jssc.201400798

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Barley seedlings are rich in flavones that can have positive effects on people with anti-hypoxia and antifatigue. Lutonarin and saponarin are two major flavonoid glycosides that have unique structures in barley seedlings. This study presents a new approach for the preparation of lutonarin and saponarin from barely seedlings by membrane separation technology and preparative high-performance liquid chromatography. Preparative conditions of these two flavonoid glycosides by membrane separation technology were studied using response surface methodology. Under the optimized conditions, the total contents of these two flavonoid glycosides amounts to 17.0%.

引用

页码：3760 / 3766

页数：7

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