N,N′-bis(benzamidothiocarbonyl)hydrazine dimethyl sulfoxide disolvate

被引：5

作者：

Yamin, BM ^{[1
]}

Yusof, MSM ^{[1
]}

机构：

[1] Univ Kebangsaan Malaysia, Sch Chem Sci & Food Technol, Bangi 43600, Selangor, Malaysia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2003年 / 59卷

关键词：

D O I：

10.1107/S1600536803003635

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, C16H14N4O2S2.2C(2)H(6)OS, the molecule is discrete and centrosymmetric. The benzoylthiuourea and benzoyl groups are cis and trans, respectively, to the thiourea S atom across the C-N bonds. In the crystal structure, the molecule is linked to the solvent DMSO molecules by N-H...O hydrogen bonds.

引用

页码：O358 / O359

页数：2

共 8 条

[1] Synthesis and structures of two N,N′-bis(2-pyridinyl)thioureas and N-(2-pyridinyl)-N′-(benzoyl)thiourea [J].

Kaminsky, W ;

Goldberg, KI ;

West, DX .

JOURNAL OF MOLECULAR STRUCTURE, 2002, 605 (01) :9-15

[2]

Nardelli M., 1995, J APPL CRYSTALLOGR, V28, P659, DOI [10.1107/S0021889895007138, DOI 10.1107/S0021889895007138]

[3]

Sheldrick G.M., 1996, SADABS VERSION 2008

[4]

Sheldrick G.M., 1997, SHELXTL VERSION 5 1

[5]

*SIEM AN XRAY INST, 1986, SMART SAINT

[6]

Spek A., 1990, ACTA CRYSTALLOGR, V46

[7] N-Benzoyl-N′-(2,6-dimethylphenyl)thiourea [J].

Usman, A ;

Razak, IA ;

Satar, S ;

Kadir, MA ;

Yamin, BM ;

Fun, HK .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2002, 58 :O656-O658

[8] N-Benzoyl-N′-phenylthiourea [J].

Yamin, BM ;

Yusof, MSM .

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2003, 59 :O151-O152

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