HT-LSCM as a Tool for Indirect Determination of Precipitates by Real-Time Grain Growth Observations

被引:3
作者
Fuchs, Nora [1 ]
Bernhard, Christian [1 ]
Michelic, Susanne [1 ]
Dippenaar, Rian [2 ]
机构
[1] Univ Leoben, Chair Ferrous Met, A-8700 Leoben, Austria
[2] Univ Wollongong, Sch Mech Mat Mechatron & Biomed Engn, Wollongong, NSW 2522, Australia
来源
TMS 2020 149TH ANNUAL MEETING & EXHIBITION SUPPLEMENTAL PROCEEDINGS | 2020年
关键词
HT-LSCM; Grain growth; Precipitation kinetics; Aluminum nitride; ALUMINUM NITRIDE; AUSTENITE; BOUNDARY; KINETICS; STEELS; SIZE;
D O I
10.1007/978-3-030-36296-6_5
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The characterization of precipitation populations in steel with respect to their size distribution or volume fraction is still a challenge for even highly sophisticated analytical methods, and hence statistical data-absolutely essential for the verification of precipitation calculations-is still rare. The present paper aims at the use of high-temperature laser scanning confocal microscopy (HT-LSCM) in situ grain growth observations for the indirect conclusion on the precipitation or dissolution of A1N depending on initial aluminium and nitrogen content and thermal cycle. A formerly developed austenite grain growth model is applied to estimate the time-dependent Zener pinning and the results are finally used to adjust the relevant input parameters for the simulation of A1N precipitation kinetics in the commercial software MatCalc. The proposed paper will present first results and discuss the potential and limits of this efficient and time saving indirect method.
引用
收藏
页码:47 / 55
页数:9
相关论文
共 20 条
[1]   ANALYTICAL MODELING OF GRAIN-GROWTH IN METALS AND ALLOYS IN THE PRESENCE OF GROWING AND DISSOLVING PRECIPITATES .1. NORMAL GRAIN-GROWTH [J].
ANDERSEN, I ;
GRONG, O .
ACTA METALLURGICA ET MATERIALIA, 1995, 43 (07) :2673-2688
[2]   DETERMINATION OF ALUMINUM NITRIDE NITROGEN IN STEEL [J].
BEEGHLY, HF .
ANALYTICAL CHEMISTRY, 1949, 21 (12) :1513-1519
[3]   EFFECTS OF 2ND-PHASE PARTICLES ON COARSENING OF AUSTENITE IN 0.15 PCT CARBON-STEELS [J].
BEPARI, MA .
METALLURGICAL TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 1989, 20 (01) :13-16
[4]   A Model for Predicting the Austenite Grain Size at the Surface of Continuously-Cast Slabs [J].
Bernhard, Christian ;
Reiter, Juergen ;
Presslinger, Hubert .
METALLURGICAL AND MATERIALS TRANSACTIONS B-PROCESS METALLURGY AND MATERIALS PROCESSING SCIENCE, 2008, 39 (06) :885-895
[5]   Revealing austenite grain boundaries by thermal etching:: advantages and disadvantages [J].
de Andrés, CG ;
Caballero, FG ;
Capdevila, C ;
San Martín, D .
MATERIALS CHARACTERIZATION, 2002, 49 (02) :121-127
[6]   Delta-ferrite recovery structures in low-carbon steels [J].
Dippenaar, RJ ;
Phelan, DJ .
METALLURGICAL AND MATERIALS TRANSACTIONS B-PROCESS METALLURGY AND MATERIALS PROCESSING SCIENCE, 2003, 34 (05) :495-501
[7]  
Fuchs N., 2015, B. Huttenmann. Monatsh., V160, P214, DOI [10.1007/s00501-015-0356-3, DOI 10.1007/S00501-015-0356-3]
[8]   Analysis of the austenite grain size distribution in plain carbon steels [J].
Giumelli, AK ;
Militzer, M ;
Hawbolt, EB .
ISIJ INTERNATIONAL, 1999, 39 (03) :271-280
[9]   THE DEFORMATION AND AGEING OF MILD STEEL .3. DISCUSSION OF RESULTS [J].
HALL, EO .
PROCEEDINGS OF THE PHYSICAL SOCIETY OF LONDON SECTION B, 1951, 64 (381) :747-753
[10]   Precipitation of aluminum nitride in a high strength maraging steel with low nitrogen content [J].
Jeanmaire, G. ;
Dehmas, M. ;
Redjaiemia, A. ;
Puech, S. ;
Fribourg, G. .
MATERIALS CHARACTERIZATION, 2014, 98 :193-201