Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

被引：25

作者：

Liermann, H. P. ^{[1
]}

Konopkova, Z. ^{[2
]}

Appel, K. ^{[2
]}

Prescher, C. ^{[1
]}

Schropp, A. ^{[1
]}

Cerantola, V ^{[2
]}

Husband, R. J. ^{[1
]}

McHardy, J. D. ^{[3
]}

McMahon, M., I ^{[3
]}

McWilliams, R. S. ^{[3
]}

Pepin, C. M. ^{[4
,5
]}

Mainberger, J. ^{[1
]}

Roeper, M. ^{[1
]}

Berghaeuser, A. ^{[6
]}

Damker, H. ^{[1
]}

Talkovski, P. ^{[1
]}

Foese, M. ^{[1
]}

Kujala, N. ^{[2
]}

Ball, O. B. ^{[3
]}

Baron, M. A. ^{[7
]}

Briggs, R. ^{[8
]}

Bykov, M. ^{[9
]}

Bykova, E. ^{[9
]}

Chantel, J. ^{[10
]}

Coleman, A. L. ^{[8
]}

Cynn, H. ^{[8
]}

Dattelbaum, D. ^{[11
]}

Dresselhaus-Marais, L. E. ^{[8
]}

Eggert, J. H. ^{[8
]}

Ehm, L. ^{[12
]}

Evans, W. J. ^{[8
]}

Fiquet, G. ^{[7
]}

Frost, M. ^{[13
]}

Glazyrin, K. ^{[1
]}

Goncharov, A. F. ^{[9
]}

Hwang, H. ^{[14
]}

Jenei, Zs ^{[8
]}

Kim, J. Y. ^{[15
]}

Langenhorst, F. ^{[16
]}

Lee, Y. ^{[14
]}

Makita, M. ^{[2
]}

Marquardt, H. ^{[17
]}

McBride, E. E. ^{[13
]}

Merkel, S. ^{[10
]}

Morard, G. ^{[7
,18
]}

O'Bannon, E. F., III ^{[8
]}

Otzen, C. ^{[1
,16
]}

Pace, E. J. ^{[3
]}

Pelka, A. ^{[5
,6
]}

Pigott, J. S. ^{[11
,19
]}

机构：

[1] Deutsch Elektronen Synchrotron DESY, Photon Sci, Notkestr 85, Hamburg, Germany

[2] European Xray Free Electron Laser Facil GmbH, Holzkoppel 4, D-22869 Schenefeld, Germany

[3] Univ Edinburgh, Ctr Sci Extreme Condit, Sch Phys & Astron, Peter Guthrie Tait Rd, Edinburgh EH9 3FD, Midlothian, Scotland

[4] CEA, DAM, DIF, F-91297 Arpajon, France

[5] Univ Paris Saclay, CEA, Lab Matiere Condit Extremes, F-91680 Bruyeres Le Chatel, France

[6] Helmholtz Zentrum Dresden Rossendorf eV, D-01328 Dresden, Germany

[7] Sorbonne Univ, Inst Mineral Phys Mat & Cosmochim IMPMC, Musee Natl dHist Nat, UMR CNRS 7590, 4 Pl Jussieu, Paris, France

[8] Lawrence Livermore Natl Lab, 7000 East Ave, Livermore, CA 94550 USA

[9] Earth & Planets Lab, Carnegie Sci, 5241 Broad Branch Rd NW, Washington, DC 20015 USA

[10] Univ Lille, CNRS, Cent Lille, UMR 8207 UMET Unite Mat & Transformat,INRAE, F-59000 Lille, France

[11] Los Alamos Natl Lab, Los Alamos, NM 87545 USA

[12] SUNY Stony Brook, Mineral Phys Inst, Stony Brook, NY 11794 USA

[13] SLAC Natl Accelerator Lab, 2575 Sand Hill Rd, Menlo Pk, CA 94025 USA

[14] Yonsei Univ, Dept Earth Syst Sci, 50 Yonsei Ro, Seoul 03722, South Korea

[15] Hanyang Univ, Res Inst High Pressure, Dept Phys, 222 Wangsimni Ro, Seoul 04763, South Korea

[16] Friedrich Schiller Univ Jena, Inst Geosci, Carl Zeiss Promenade 10, D-07745 Jena, Germany

[17] Univ Oxford, Dept Earth Sci, South Pk Rd, Oxford OX1 3AN, England

[18] Univ Grenoble Alpes, Univ Savoie Mt Blanc, CNRS, IRD,IFSTTAR,ISTerre, F-38000 Grenoble, France

[19] Case Western Reserve Univ, 10900 Euclid Ave, Cleveland, OH 44106 USA

[20] Univ Chicago, Ctr Adv Radiat Sources, Chicago, IL 60637 USA

[21] Univ Rostock, Inst Phys, D-18051 Rostock, Germany

[22] Univ Munster, Inst Mineral, Munster, Germany

[23] GFZ German Res Ctr Geosci, Telegrafenberg, D-14473 Potsdam, Germany

[24] Univ Potsdam, Inst Geowissensch, Karl Liebknecht Str 24-25, D-14476 Potsdam, Germany

[25] Washington State Univ, Inst Shock Phys & Mat Sci & Engn, Dept Chem, Pullman, WA 99164 USA

来源：

JOURNAL OF SYNCHROTRON RADIATION | 2021年 / 28卷 / 28期

基金：

英国工程与自然科学研究理事会; 欧洲研究理事会; 欧盟地平线“2020”; 美国国家科学基金会;

关键词：

diamond anvil cells; X-ray free-electron lasers; high-precision X-ray diffraction; finite element modeling; HIGH-PRESSURE;

D O I：

10.1107/S1600577521002551

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

The high-precision X-ray diffraction setup for work with diamond anvil cells (DAC5) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump-probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.

引用

页码：688 / 706

页数：19

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