New method for preparation of low oxygen Mo powder by reduction of MoO3 using Ca

被引:7
作者
Oh, J. -M. [1 ]
Kim, W. [1 ]
Lee, B. -K. [1 ]
Suh, C. -Y. [1 ]
Kim, H. -S. [1 ]
Lim, J. -W. [2 ]
机构
[1] Korea Inst Geosci & Mineral Resources, Mineral Resources Res Div, Taejon 305350, South Korea
[2] Chonbuk Natl Univ, Coll Engn, Div Adv Mat Engn, Jeonju 561756, South Korea
关键词
Molybdenum; Powder; Oxygen; Reduction; Deoxidation; HYDROGEN-REDUCTION; CALCIOTHERMIC REDUCTION; MOLYBDENUM OXIDES; PRESSURE; BEHAVIOR; INGOT; METAL;
D O I
10.1179/1743290113Y.0000000083
中图分类号
TF [冶金工业];
学科分类号
0806 ;
摘要
A new method for the reduction of MoO3 using Ca as a reducing agent was developed. A low oxygen Mo powder can thus be prepared by two-step reduction process: the first step reduction involves a contact type method while the second step reduction uses a non-contact type method involving Ca vapour followed by additional deoxidation. The oxygen concentration in the resultant Mo powder was similar to 2800 ppm, which was much lower than that of commercial Mo powder (>4400 ppm).
引用
收藏
页码:291 / 294
页数:4
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