Isotropic and anisotropic chemical shift in 207Pb NMR of inorganic solids

被引：4

作者：

Fayon, F ^{[1
]}

Bessada, C

Massiot, D

Farnan, I

Coutures, JP

机构：

[1] CNRS, Ctr Rech Phys Hautes Temp, F-45071 Orleans 2, France

[2] Univ Cambridge, Dept Earth Sci, Cambridge CB2 3EQ, England

来源：

JOURNAL DE CHIMIE PHYSIQUE ET DE PHYSICO-CHIMIE BIOLOGIQUE | 1998年 / 95卷 / 02期

关键词：

NMR; Pb-207; chemical shift; correlation;

D O I：

10.1051/jcp:1998138

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

We have recently described empirical correlations between Pb-207 NMR chemical shift (oxidation state 2+) and structure in solids (Fayon et al.) that should allow the use of Pb-207 NMR as a structural probe in disordered solids of complex composition. These empirical correlations are compared to new experimental NMR data in crystalline lead aluminates and lead silicates.

引用

页码：317 / 321

页数：5

共 9 条

[1] Empirical correlations between Pb-207 NMR chemical shifts and structure in solids [J].

Fayon, F ;

Farnan, I ;

Bessada, C ;

Coutures, J ;

Massiot, D ;

Coutures, JP .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1997, 119 (29) :6837-6843

[2] SIDEBAND INTENSITIES IN NMR-SPECTRA OF SAMPLES SPINNING AT THE MAGIC ANGLE [J].

HERZFELD, J ;

BERGER, AE .

JOURNAL OF CHEMICAL PHYSICS, 1980, 73 (12) :6021-6030

[3] SOLID-STATE PB-207 CP-MAS NMR OF LEAD(II) COMPOUNDS FOR THE STRUCTURAL STUDY OF MOLECULAR ROUTES TO LEAD-BASED PEROVSKITE-PHASE MATERIALS [J].

IRWIN, AD ;

CHANDLER, CD ;

ASSINK, R ;

HAMPDENSMITH, MJ .

INORGANIC CHEMISTRY, 1994, 33 (06) :1005-1006

[4] NMR IN LEAD-CONTAINING COMPOUNDS [J].

KIM, KS ;

BRAY, PJ .

JOURNAL OF MAGNETIC RESONANCE, 1974, 16 (02) :334-338

[5] CONVENTIONS FOR THE REPORTING OF NUCLEAR MAGNETIC SHIELDING (OR SHIFT) TENSORS SUGGESTED BY PARTICIPANTS IN THE NATO ARW ON NMR SHIELDING CONSTANTS AT THE UNIVERSITY-OF-MARYLAND, COLLEGE-PARK, JULY 1992 [J].

MASON, J .

SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1993, 2 (05) :285-288

[6] Determination of Pb-207(2+) chemical shift tensors from precise powder lineshape analysis [J].

Neue, G ;

Dybowski, C ;

Smith, ML ;

Hepp, MA ;

Perry, DL .

SOLID STATE NUCLEAR MAGNETIC RESONANCE, 1996, 6 (03) :241-250

[7] NMR CHEMICAL SHIFTS OF PB-207 IN A FEW COMPOUNDS [J].

PIETTE, LH ;

WEAVER, HE .

JOURNAL OF CHEMICAL PHYSICS, 1958, 28 (04) :735-736

[8] CORRELATION OF SI-O-SI OR SI-O-AL ANGLES AND SI-29 NMR CHEMICAL-SHIFTS IN SILICATES AND ALUMINOSILICATES - INTERPRETATION BY SEMI-EMPIRICAL QUANTUM-CHEMICAL CONSIDERATIONS [J].

RADEGLIA, R ;

ENGELHARDT, G .

CHEMICAL PHYSICS LETTERS, 1985, 114 (01) :28-30

[9] STRUCTURE AND CATION EFFECTS ON P-31 NMR CHEMICAL-SHIFTS AND CHEMICAL-SHIFT ANISOTROPIES OF ORTHO-PHOSPHATES [J].

TURNER, GL ;

SMITH, KA ;

KIRKPATRICK, RJ ;

OLDFIELD, E .

JOURNAL OF MAGNETIC RESONANCE, 1986, 70 (03) :408-415

← 1 →