共 35 条
Selective synthesis of Fe3O4, γ-Fe2O3, and α-Fe2O3 using cellulose-based composites as precursors
被引:83
作者:

Liu, Shan
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机构:
Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China

Yao, Ke
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h-index: 0
机构:
Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China

Fu, Lian-Hua
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h-index: 0
机构:
Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China

Ma, Ming-Guo
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h-index: 0
机构:
Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China
机构:
[1] Beijing Forestry Univ, Coll Mat Sci & Technol, Beijing Key Lab Lignocellulos Chem, Beijing 100083, Peoples R China
来源:
关键词:
IRON-OXIDE NANOPARTICLES;
IN-SITU SYNTHESIS;
THERMAL TRANSFORMATION;
IONIC-LIQUID;
NANOFIBRILLATED CELLULOSE;
NANOCOMPOSITES;
BIOSYNTHESIS;
PARTICLES;
D O I:
10.1039/c5ra22985e
中图分类号:
O6 [化学];
学科分类号:
0703 ;
摘要:
Iron oxide with various phases such as Fe3O4, gamma-Fe2O3, and alpha-Fe2O3 has been selective successfully synthesized using cellulose-based composites as precursors, which were obtained at 180 degrees C for 45 min by the microwave-hydrothermal method. The products were characterized with X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric analysis (TG), derivative thermogravimetric analysis (DTG), X-ray photoelectron spectroscopy (XPS), and scanning electron microscopy (SEM). Fe3O4, gamma-Fe2O3, and alpha-Fe2O3 could be selectively synthesized by changing the calcination temperature and atmosphere. It was found that Fe3O4 was obtained in the N-2 atmosphere. However, gamma-Fe2O3 and alpha-Fe2O3 were observed at 300 and 500 degrees C for 3 h in the air atmosphere, respectively. The as-synthesized Fe3O4 and gamma-Fe2O3 displayed superparamagnetic characteristics at room temperature via the magnetization measurement. The methylene blue (MB) adsorption capacity of gamma-Fe2O3 (air 300 degrees C) can reach 98.72% and the adsorption isotherms better fitted Freundlich isotherm models. This work provided a promising strategy for the synthesis of metal and carbon/metal composites using biomass as a precursor.
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页码:2135 / 2140
页数:6
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