Synthesis and spectroscopic characterization of nanostructured anatase titania: A photocatalyst

被引：104

作者：

Porkodi, K. ^{[1
]}

Arokiamary, S. Daisy

机构：

[1] PSG Coll Technol, Dept Chem, Coimbatore 641004, Tamil Nadu, India

[2] Sri Krishna Coll Engn & Technol, Dept Phys, Coimbatore, Tamil Nadu, India

来源：

MATERIALS CHARACTERIZATION | 2007年 / 58卷 / 06期

关键词：

nanocrystalline TiO2; sol-gel; FT-Raman; FT-IR; thermal analysis; SEM;

D O I：

10.1016/j.matchar.2006.04.019

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Nanocrystalline TiO2 was synthesized by the sol-gel process by controlling the crystallite size through calcination. The resulting nanocrystals were characterized using XRD, FT-Raman, SEM/EDX, DSC/TGA and UV-Vis spectroscopic techniques. XRD patterns confirmed the presence of only pure 100% anatase phase TiO2 The surface morphology of the nanotitania was evaluated with Scanning Electron Microscopy. The purity of the sol-gel-derived TiO2 was confirmed through EDX measurements. The band gap of the nanotitania was found to be 3.6 eV from UV-Vis measurements. The pHzpc of the titania sample was measured as 5.90. (c) 2006 Elsevier Inc. All rights reserved.

引用

页码：495 / 503

页数：9

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