HyFlex EDM: superficial features, metallurgical analysis and fatigue resistance of innovative electro discharge machined NiTi rotary instruments

被引:114
作者
Pirani, C. [1 ]
Iacono, F. [1 ]
Generali, L. [2 ]
Sassatelli, P. [3 ]
Nucci, C. [1 ]
Lusvarghi, L. [3 ]
Gandolfi, M. G. [1 ]
Prati, C. [1 ]
机构
[1] Univ Bologna, Alma Mater Studiorum, Endodont Clin Sect, Dept Biomed & Neuromotor Sci DIBINEM, Bologna, Italy
[2] Univ Modena & Reggio Emilia, Endodont Sect, Sch Dent, Dept Surg Med Dent & Morphol Sci Transplant Surg, Modena, Italy
[3] Univ Modena & Reggio Emilia, Dept Engn Enzo Ferrari DIEF, Modena, Italy
关键词
CM wire; electro discharge machining (EDM); ESEM analysis; fatigue resistance; NiTi endodontic instruments; usage-induced degradation; CONTROLLED MEMORY WIRE; NICKEL-TITANIUM INSTRUMENTS; TI ENDODONTIC INSTRUMENTS; SHAPE-MEMORY; CYCLIC FATIGUE; METALLOGRAPHIC ANALYSIS; FRACTOGRAPHIC ANALYSIS; CLINICAL-USE; ROOT CANALS; ALLOYS;
D O I
10.1111/iej.12470
中图分类号
R78 [口腔科学];
学科分类号
1003 ;
摘要
AimTo evaluate the surface and microstructural alterations of new and used HyFlex EDM prototypes and to test their fatigue resistance. MethodologyFifteen HyFlex EDM prototypes were used for invitro instrumentation of severely curved root canals. Surface and microstructural characteristics of new and used files were compared by ESEM analysis equipped with energy dispersive X-ray spectrophotometry (EDS) and optical metallographic imaging. Usage-induced degradation was assessed. Thirty additional HyFlex EDM prototypes and 20 standard manufactured HyFlex CM files were subjected to cyclic fatigue tests. Time to fracture was recorded, and results were validated using the Kruskal-Wallis test (-level 0.05). Fatigued files were analysed by ESEM for fractographic evaluation. ResultsSurface and microstructural characterization of EDM prototypes revealed the typical spark-machined surface of a NiTi EDM alloy. No fractures were registered during root canal instrumentation. No evident surface alterations and minor degradation were observed between new and used instruments. The metallographic analysis of new and used files disclosed a homogeneous structure, mostly composed of lenticular martensite grains, and some residual austenite. The cyclic fatigue test showed an increase of fatigue resistance up to 700% on the EDM compared to CM files. ConclusionsSpark-machined peculiar surface is the main feature of HyFlex EDM. Low degradation was observed after multiple canal instrumentations. Prototypes exhibited surprising high values of cyclic fatigue resistance and a safe invitro use in severely curved canals.
引用
收藏
页码:483 / 493
页数:11
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