Ptychographic X-ray computed tomography of extended colloidal networks in food emulsions

被引:11
作者
Nielsen, Mikkel Schou [1 ]
Munk, Merete Bogelund [2 ]
Diaz, Ana [3 ]
Pedersen, Emil Boje Lind [4 ]
Holler, Mirko [3 ]
Bruns, Stefan [5 ]
Risbo, Jens [2 ]
Mortensen, Kell [1 ]
Feidenhans'l, Robert [1 ]
机构
[1] Univ Copenhagen, Niels Bohr Inst, Univ Pk 5, DK-2100 Copenhagen, Denmark
[2] Univ Copenhagen, FOOD, Rolighedsvej 30, DK-2000 Frederiksberg, Denmark
[3] Paul Scherrer Inst, CH-5232 Villigen, Switzerland
[4] Tech Univ Denmark, Dept Energy Convers, Frederiksborgvej 399, DK-4000 Roskilde, Denmark
[5] Univ Copenhagen, Dept Chem, Nanosci Ctr, Univ Pk 5, DK-2100 Copenhagen, Denmark
来源
FOOD STRUCTURE-NETHERLANDS | 2016年 / 7卷
关键词
Food emulsion; Colloidal network; 3D microstructure; X-ray ptychography; Computed tomography; X-ray phase-contrast imaging;
D O I
10.1016/j.foostr.2016.01.001
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
As a main structural level in colloidal food materials, extended colloidal networks are important for texture and rheology. By obtaining the 3D microstructure of the network, macroscopic mechanical properties of the material can be inferred. However, this approach is hampered by the lack of suitable non-destructive 3D imaging techniques with submicron resolution. We present results of quantitative ptychographic X-ray computed tomography applied to a palm kernel oil based oil-in-water emulsion. The measurements were carried out at ambient pressure and temperature. The 3D structure of the extended colloidal network of fat globules was obtained with a resolution of around 300 nm. Through image analysis of the network structure, the fat globule size distribution was computed and compared to previous findings. In further support, the reconstructed electron density values were within 4% of reference values. (C) 2016 Elsevier Ltd. All rights reserved.
引用
收藏
页码:21 / 28
页数:8
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