Lard detection based on fatty acids profile using comprehensive gas chromatography hyphenated with time-of-flight mass spectrometry

被引:83
作者
Indrasti, Dias [1 ]
Man, Yaakob B. Che [1 ]
Mustafa, Shuhaimi [1 ]
Hashim, Dzulkifly Mat [1 ]
机构
[1] Univ Putra Malaysia, Halal Prod Res Inst, Serdang 43400, Selangor Darul, Malaysia
关键词
Lard; Animal fats; Fatty acid; FAME; GC x GC; TOF-MS; EDIBLE OILS; SEED OIL; MEAT; EXTRACTION; TISSUE;
D O I
10.1016/j.foodchem.2010.03.082
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Comprehensive gas chromatography hyphenated with time-of-flight mass spectrometry was applied to detect the differences between lard (LA) and three other commonly animal-derived fats, namely cattle fat (CA), chicken fat (CF) and goat fat (CF). Combination of two different microbore columns (SLB-5ms and DB-wax) allowed the discrimination of lard from other animal fats by three fatty acid methyl esters (FAMEs) constituents involving methyl trans-9,12,15-octadecatrienoate (C18:3 n3t), methyl 11,14,17-eicosatrienoate (C20:3 n3t) and methyl 11,14-eicosadienoate (C20:2 n6). The FAME profiles could be used as a basis for discriminating lard from other animal fats in food authentication process. (C) 2010 Elsevier Ltd. All rights reserved.
引用
收藏
页码:1273 / 1277
页数:5
相关论文
共 21 条
[1]   Recent developments in the application of comprehensive two-dimensional gas chromatography [J].
Adahchour, M. ;
Beens, J. ;
Brinkman, U. A. Th. .
JOURNAL OF CHROMATOGRAPHY A, 2008, 1186 (1-2) :67-108
[2]   Improved fatty acid detection in micro-algae and aquatic meiofauna species using a direct thermal desorption interface combined with comprehensive gas chromatography-time-of-flight mass spectrometry [J].
Akoto, Lawrence ;
Stellaard, Frans ;
Irth, Hubertus ;
Vreuls, Rene J. J. ;
Pel, Roel .
JOURNAL OF CHROMATOGRAPHY A, 2008, 1186 (1-2) :254-261
[3]  
Al-Bahrany AM., 2002, PAK J BIOL SCI, V5, P212, DOI DOI 10.3923/PJBS.2002.212.214
[4]   Muslim consumer trust in halal meat status and control in Belgium [J].
Bonne, Karijn ;
Verbeke, Wim .
MEAT SCIENCE, 2008, 79 (01) :113-123
[5]   Simultaneous determination of total lipid, cholesterol and fatty acids in meat and backfat of suckling and adult pigs [J].
Bragagnolo, N ;
Rodriguez-Amaya, DB .
FOOD CHEMISTRY, 2002, 79 (02) :255-260
[6]   Comprehensive two-dimensional gas chromatograpy with time-of-flight mass spectrometric detection applied to the determination of pesticides in food extracts [J].
Dallüge, J ;
van Rijn, M ;
Beens, J ;
Vreuls, RJJ ;
Brinkman, UAT .
JOURNAL OF CHROMATOGRAPHY A, 2002, 965 (1-2) :207-217
[7]   Comprehensive two-dimensional gas chromatography:: a powerful and versatile analytical tool [J].
Dallüge, J ;
Beens, J ;
Brinkman, UAT .
JOURNAL OF CHROMATOGRAPHY A, 2003, 1000 (1-2) :69-108
[8]  
de Koning S, 2006, LC GC EUR, V19, P590
[9]  
DEMAN JM, 1999, FUNCTIONALITIES REQU
[10]   Microwave oven application in the extraction of fat from the subcutaneous tissue of Iberian pig ham [J].
DePedro, E ;
Casillas, M ;
Miranda, CM .
MEAT SCIENCE, 1997, 45 (01) :45-51