Damage of Semicrystalline Polyamide 6 Assessed by 3D X-Ray Tomography: From Microstructural Evolution to Constitutive Modeling

被引：44

作者：

Laiarinandrasana, L. ^{[1
]}

Morgeneyer, T. F. ^{[1
]}

Proudhon, H. ^{[1
]}

Regrain, C. ^{[1
]}

机构：

[1] CNRS, Ctr Mat, MINES Paristech, UMR 7633, F-91003 Evry, France

来源：

JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS | 2010年 / 48卷 / 13期

关键词：

creep; damage zone; fracture; mechanical properties; modeling; necking; polyamides; porosity; semicrystalline polymers; tensile tests; voids; X-ray tomography; POLYVINYLIDENE FLUORIDE; DEFORMATION; CAVITATION; SCATTERING; POLYMERS; GROWTH; METALS;

D O I：

10.1002/polb.22043

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

In this study an attempt is made to link the damage and microstructural evolution of semicrystalline polymers, in particular polyamide 6, to the macroscopic material behavior during tensile and creep tests. Tensile specimens, removed before failure were seen to have undergone striction. They were examined using synchrotron radiation tomography. These samples showed elongated axisymmetric columns of voids separated by thin ligaments of material. These observations were confirmed and refined through a cryofractography experiment of a different tensile sample, stopped before failure. An attempt was made to obtain quantitative data about void volume fraction and morphology through image analysis. (C) 2010 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 48: 1516-1525, 2010

引用

页码：1516 / 1525

页数：10

共 50 条

[1] Damage evolution in TWIP and standard austenitic steel by means of 3D X ray tomography
Fabregue, D.
Landron, C.
Bouaziz, O.
Maire, E.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2013, 579 : 92 - 98
[2] Comparison of Damage Evolution in Different Steels by Means of 3D X Ray Tomography
Fabregue, Damien
Landron, Caroline
Bouaziz, Olivier
Maire, Eric
STEEL RESEARCH INTERNATIONAL, 2015, 86 (10) : 1197 - 1203
[3] 3D microstructural evolution in sintering observed by X-ray microtomography
Okuma, Gaku
JOURNAL OF THE CERAMIC SOCIETY OF JAPAN, 2023, 131 (09) : 522 - 532
[4] Effect of Multiaxial Stress State on Morphology and Spatial Distribution of Voids in Deformed Semicrystalline Polymer Assessed by X-ray Tomography
Laiarinandrasana, Lucien
Morgeneyer, Thilo F.
Proudhon, Henry
N'guyen, Franck
Maire, Eric
MACROMOLECULES, 2012, 45 (11) : 4658 - 4668
[5] 3D microstructural characterization and mechanical properties of constituent particles in Al 7075 alloys using X-ray synchrotron tomography and nanoindentation
Singh, Sudhanshu S.
Schwartzstein, Cary
Williams, Jason J.
Xiao, Xianghui
De Carlo, Francesco
Chawla, Nikhilesh
JOURNAL OF ALLOYS AND COMPOUNDS, 2014, 602 : 163 - 174
[6] 3D visualization of defects and microstructural features with laboratory-scale X-ray tomography apparatuses
2013, Japan Institute of Light Metals (63): : 343 - 349
[7] Damage evolution in SiC/SiC unidirectional composites by X-ray tomography
Hilmas, Ashley M.
Sevener, Kathleen M.
Halloran, John W.
JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2020, 103 (05) : 3436 - 3447
[8] Phase Transformation and Microstructural Evolution of CuS Electrodes in Solid-State Batteries Probed by In Situ 3D X-Ray Tomography
Zhang, Zhenggang
Dong, Kang
Mazzio, Katherine A.
Hilger, Andre
Markoetter, Henning
Wilde, Fabian
Heinemann, Tobias
Manke, Ingo
Adelhelm, Philipp
ADVANCED ENERGY MATERIALS, 2023, 13 (02)
[9] Observations by in-situ X-ray synchrotron computed tomography of the microstructural evolution of semi-crystalline Polyamide 11 during deformation
Poulet, Pierre-Alexis
Hochstetter, Gilles
King, Andrew
Proudhon, Henry
Joannes, Sebastien
Laiarinandrasana, Lucien
POLYMER TESTING, 2016, 56 : 245 - 260
[10] Microstructural characterization and constitutive modeling of deformation of closed-cell foams based on in situ x-ray tomography
Chai, H. W.
Xie, Z. L.
Xiao, X. H.
Xie, H. L.
Huang, J. Y.
Luo, S. N.
INTERNATIONAL JOURNAL OF PLASTICITY, 2020, 131

← 1 2 3 4 5 →