New approach for the detection of organophosphorus pesticide in cabbage using SPME/SnO2 gas sensor:: principle and preliminary experiment

被引:10
作者
Huang, XJ
Sun, YF
Meng, FL
Liu, JH [1 ]
机构
[1] Chinese Acad Sci, Hefei Inst Intelligent Machines, Hefei 230031, Peoples R China
[2] Univ Sci & Technol China, Dept Chem, Hefei 230026, Peoples R China
基金
中国国家自然科学基金;
关键词
SPME/SnO2; gas sensor; organophosphate pesticide; fast detection;
D O I
10.1016/j.snb.2004.04.025
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A new approach for fast detection of organophosphorus pesticide like dichlorvos in cabbage using solid phase microextraction (SPME) coupled with tin dioxide gas sensor was investigated. In comparison the experiments of guide sample of dichlorvos, this method which employed only one SnO2 gas sensor rather than an array of sensors in a rectangular temperature mode could perform the qualitative analysis. The quantitative analysis was performed using polar plots and peak area. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:235 / 240
页数:6
相关论文
共 20 条
[1]   Optimization of solid-phase microextraction conditions using a response surface methodology to determine organochlorine pesticides in water by gas chromatography and electron-capture detection [J].
Aguilar, C ;
Peñalver, A ;
Pocurull, E ;
Ferré, J ;
Borrull, F ;
Marcé, RM .
JOURNAL OF CHROMATOGRAPHY A, 1999, 844 (1-2) :425-432
[2]   Solid-phase microextraction in pesticide residue analysis [J].
Beltran, J ;
López, FJ ;
Hernández, F .
JOURNAL OF CHROMATOGRAPHY A, 2000, 885 (1-2) :389-404
[3]   Solid-phase microextraction method for the determination of atrazine and four organophosphorus pesticides in soil samples by gas chromatography [J].
Bouaid, A ;
Ramos, L ;
Gonzalez, MJ ;
Fernández, P ;
Cámara, C .
JOURNAL OF CHROMATOGRAPHY A, 2001, 939 (1-2) :13-21
[4]   Determination of chlorinated pesticides in water by SPME/GC [J].
Boussahel, R ;
Bouland, S ;
Moussaoui, KM ;
Baudu, M ;
Montiel, A .
WATER RESEARCH, 2002, 36 (07) :1909-1911
[5]   Effect of the various parameters governing solid-phase microextraction for the trace-determination of pesticides in water [J].
Dugay, J ;
Miège, C ;
Hennion, MC .
JOURNAL OF CHROMATOGRAPHY A, 1998, 795 (01) :27-42
[6]   ELEMENT-SELECTIVE DETECTION OF PESTICIDES BY GAS-CHROMATOGRAPHY ATOMIC-EMISSION DETECTION AND SOLID-PHASE MICROEXTRACTION [J].
EISERT, R ;
LEVSEN, K ;
WUNSCH, G .
JOURNAL OF CHROMATOGRAPHY A, 1994, 683 (01) :175-183
[7]   Determination of organophosphorus pesticides in honeybees after solid-phase microextraction [J].
Fernández, M ;
Padrón, C ;
Marconi, L ;
Ghini, S ;
Colombo, R ;
Sabatini, AG ;
Girotti, S .
JOURNAL OF CHROMATOGRAPHY A, 2001, 922 (1-2) :257-265
[8]   Analysis of acidic pesticides using in situ derivatization with alkylchloroformate and solid-phase microextraction (SPME) for GC-MS [J].
Henriksen, T ;
Svensmark, B ;
Lindhardt, B ;
Juhler, RK .
CHEMOSPHERE, 2001, 44 (07) :1531-1539
[9]   Solid phase microextraction associated with microwave assisted extraction of organochlorine pesticides in medicinal plants [J].
Ho, WH ;
Hsieh, SJ .
ANALYTICA CHIMICA ACTA, 2001, 428 (01) :111-120
[10]   Quantitative analysis of pesticide residue based on the dynamic response of a single SnO2 gas sensor [J].
Huang, XJ ;
Wang, LC ;
Sun, YF ;
Meng, FL ;
Liu, JH .
SENSORS AND ACTUATORS B-CHEMICAL, 2004, 99 (2-3) :330-335