Novel Schiff base ligand-assisted in-situ synthesis of Cu3V2O8 nanoparticles via a simple precipitation approach

被引:75
作者
Ghiyasiyan-Arani, Maryam [1 ]
Masjedi-Arani, Maryam [2 ]
Salavati-Niasari, Masoud [1 ]
机构
[1] Univ Kashan, Inst Nano Sci & Nano Technol, POB 87317-51167, Kashan, Iran
[2] Islamic Azad Univ, Arak Branch, Young Researchers & Elite Club, Arak, Iran
基金
美国国家科学基金会;
关键词
Nanostructure; Chemical synthesis; Photocatalytic activity; Magnetic property; Optical property; Electron microscopy; OPTICAL-PROPERTIES; TIO2; NI; CO;
D O I
10.1016/j.molliq.2015.12.100
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The effect of different Schiff-base ligands on size, morphology and uniformity of Cu3V2O8 nanoparticles prepared via a simple in-situ precipitation route was investigated. Different calcination temperatures were applied and the as-prepared products were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared (FT-IR) spectrum, Electron Dispersive X-ray spectroscopy (EDX) and ultraviolet-visible (UV-Vis) spectroscopy. Vibrating sample magnetometer (VSM) was used to study the magnetism properties of Cu3V2O8 sample. According to the obtained results, using the appropriate amount of Schiff-base ligand is a crucial parameter for the control in particle size. The photocatalytic activity of Cu3V2O8 nanostructures was evaluated by the degradation of methylene blue in aqueous solution under UV and visible light irradiation. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码:59 / 66
页数:8
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