Fast and adjustable-resolution grazing-incidence x-ray liquid surface diffraction

被引:28
作者
Fontaine, P [1 ]
Goldmann, M [1 ]
Bordessoule, M [1 ]
Jucha, A [1 ]
机构
[1] Ctr Univ Paris Sud, CNRS, UMR 130, LURE, F-91898 Orsay, France
关键词
D O I
10.1063/1.1790582
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
We developed a configuration using a two-dimensional detector for grazing incidence x-ray diffraction on Langmuir monolayers and, more generally, for surface diffraction on two-dimensional powders. Compared to the classical setup using a linear detector combined with Soller slits, the acquisition time is reduced by an order of magnitude (from more than 1 h to a few minutes) using the same x-ray source (synchrotron bending magnet) with a comparable signal to noise ratio. Moreover, experimental resolution can be adjusted by varying a vertical slit (horizontal gap) and, for small values of the gap, better resolution can be achieved compared to the one obtained with the Soller slits and linear detector. (C) 2004 American Institute of Physics.
引用
收藏
页码:3097 / 3106
页数:10
相关论文
共 35 条
[1]  
Als-Nielsen J, 1991, HDB SYNCHROTRON RAD, V4
[2]   MELTING OF SHORT 1-ALCOHOL MONOLAYERS ON WATER - THERMODYNAMICS AND X-RAY-SCATTERING STUDIES [J].
BERGE, B ;
KONOVALOV, O ;
LAJZEROWICZ, J ;
RENAULT, A ;
RIEU, JP ;
VALLADE, M ;
ALSNIELSEN, J ;
GRUBEL, G ;
LEGRAND, JF .
PHYSICAL REVIEW LETTERS, 1994, 73 (12) :1652-1655
[3]  
BOHM C, 1993, BIOPHYS J, V64, P553, DOI 10.1016/S0006-3495(93)81386-9
[4]   A simplified read out for high-resolution linear gas detector [J].
Bordessoule, M ;
Bartol, F ;
Lemonnier, M ;
Santiard, JC .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 1997, 390 (1-2) :79-85
[5]   High-resolution x-ray scattering measurements: I. Surfaces [J].
Daillant, J ;
Alba, M .
REPORTS ON PROGRESS IN PHYSICS, 2000, 63 (10) :1725-1777
[6]  
Daillant J., 1999, XRAY NEUTRON REFLECT
[7]   X-RAY-DIFFRACTION STUDIES OF ORGANIC MONOLAYERS ON THE SURFACE OF WATER [J].
DUTTA, P ;
PENG, JB ;
LIN, B ;
KETTERSON, JB ;
PRAKASH, M ;
GEORGOPOULOS, P ;
EHRLICH, S .
PHYSICAL REVIEW LETTERS, 1987, 58 (21) :2228-2231
[8]   Influence of headgroup cross-linking on chain packing in Langmuir monolayers of n-alkyltrialkoxysilanes [J].
Fontaine, P ;
Goldmann, M ;
Rondelez, F .
LANGMUIR, 1999, 15 (04) :1348-1352
[9]   Grazing incidence X-ray diffraction studies of thin films using an imaging plate detection system [J].
Foran, GJ ;
Peng, JB ;
Steitz, R ;
Barnes, GT ;
Gentle, IR .
LANGMUIR, 1996, 12 (03) :774-777
[10]   Time-resolved grazing-incidence diffraction studies of thin films using an imaging-plate camera and focusing monochromator [J].
Foran, GJ ;
Gentle, IR ;
Garrett, RF ;
Creagh, DC ;
Peng, JB ;
Barnes, GT .
JOURNAL OF SYNCHROTRON RADIATION, 1998, 5 :107-111