An interlaboratory study on passive sampling of emerging water pollutants

被引：40

作者：

Vrana, Branislav ^{[1
,2
]}

Smedes, Foppe ^{[1
,3
]}

Prokes, Roman ^{[1
]}

Loos, Robert ^{[4
]}

Mazzella, Nicolas ^{[5
]}

Miege, Cecile ^{[6
]}

Budzinski, Helene ^{[7
]}

Vermeirssen, Etienne ^{[8
,9
]}

Ocelka, Tomas ^{[10
,11
]}

Gravell, Anthony ^{[12
]}

Kaserzon, Sarit ^{[13
]}

机构：

[1] Masaryk Univ, Fac Sci, Res Ctr Tox Cpds Environm RECETOX, Kamenice 753-5, Brno 62500, Czech Republic

[2] Water Res Inst, Nabr Arm Gen L Svobodu 5, Bratislava 81249, Slovakia

[3] Deltares, POB 85467, NL-3508 AL Utrecht, Netherlands

[4] EuropeanCommiss DG Joint Res Ctr JRC, IES, Via Enrico Fermi 2749,TP 290, I-21027 Ispra, VA, Italy

[5] IRSTEA, 3 Bis Quaff Chauveau,CP 220, F-69336 Lyon, France

[6] IRSTEA, 50 Ave Verdun, F-33612 Cestas, France

[7] Univ Bordeaux 1, CNRS, UMR 5255, EPOC LPTC, 351 Crs Liberat, F-33405 Talence, France

[8] Eawag EPFL, Swiss Ctr Appl Ecotoxicol, CH-8600 Dubendorf, Switzerland

[9] Eawag, Swiss Fed Inst Aquat Sci & Technol, CH-8600 Dubendorf, Switzerland

[10] Inst Publ Hlth, Partyzanske Nam 7, Ostrava 70200, Czech Republic

[11] Environm & Hlth Serv, Zitna 1633-47, Prague 12000, Czech Republic

[12] Nat Resources Wales Llanelli Lab, 19 Penyfai Lane, Llanelli SA15 4EL, Wales

[13] Univ Queensland, Natl Res Ctr Environm Toxicol Entox, 39 Kessels Rd, Coopers Plains, Qld 4108, Australia

来源：

TRAC-TRENDS IN ANALYTICAL CHEMISTRY | 2016年 / 76卷

关键词：

Brominated diphenyl ether; Fluorinated surfactant; Emerging pollutant; Interlaboratory study; Pharmaceutical; Polar pesticide; Passive sampling; Steroid hormone; Water analysis; POLYCYCLIC AROMATIC-HYDROCARBONS; PERFORMANCE REFERENCE COMPOUNDS; POLYCHLORINATED-BIPHENYLS; SAMPLERS; COEFFICIENTS; DEVICES;

D O I：

10.1016/j.trac.2015.10.013

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

An inter-laboratory study was organised for the monitoring of emerging aquatic pollutants (pharmaceuticals, pesticides, steroids, brominated diphenyl ethers and others) using passive samplers. Thirty laboratories participated in the sampler comparison exercise. Various samplers designs were exposed at a single sampling site to treated waste water. The organisers deployed in parallel multiple samplers of a single type, which were distributed for evaluation of the contribution of the different analytical procedures to the data variability. Between laboratory variation of results from passive samplers was about factor 5 larger than within laboratory variability. Similar results obtained for different passive samplers analysed by individual laboratories and also low within laboratory variability indicate that the passive sampling process is causing less variability than the analysis. Concentrations in composite water samples were within the range obtained by passive samplers. In future a significant improvement of analytical precision and calibration of adsorption based passive samplers is needed. (C) 2015 Elsevier B.V. All rights reserved.

引用

页码：153 / 165

页数：13

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