4-{3-[Hydroxy(phenyl)methyl]-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-4-yl}benzenesulfonamide

被引:2
作者
Akkurt, Mehmet [1 ]
Celik, Ismail [2 ]
Cihan, Goekce [3 ]
Capan, Gueltaze [3 ]
Buyukgungor, Orhan [4 ]
机构
[1] Erciyes Univ, Fac Arts & Sci, Dept Phys, TR-38039 Kayseri, Turkey
[2] Cumhuriyet Univ, Fac Arts & Sci, Dept Phys, TR-58140 Sivas, Turkey
[3] Istanbul Univ, Fac Pharm, Dept Pharmaceut Chem, TR-34116 Istanbul, Turkey
[4] Ondokuz Mayis Univ, Fac Arts & Sci, Dept Phys, TR-55139 Kurupelit, Turkey
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2010年 / 66卷
关键词
DERIVATIVES;
D O I
10.1107/S1600536810011402
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C15H14N4O3S2, the hydroxy group is disordered over two positions with occupancies of 0.619 (5) and 0.381 (5). The benzene ring attached to the heterocycle makes a dihedral angle of 86.92 (9)degrees with respect to the best plane through the five-membered ring. The crystal packing is stabilized by intermolecular O-H center dot center dot center dot O, N-H center dot center dot center dot S, N-H center dot center dot center dot N, C-H center dot center dot center dot O and C-H center dot center dot center dot N hydrogen bonds, and N-H center dot center dot center dot pi and C-H center dot center dot center dot pi interactions.
引用
收藏
页码:O974 / U3507
页数:13
相关论文
共 12 条
  • [1] SIR97:: a new tool for crystal structure determination and refinement
    Altomare, A
    Burla, MC
    Camalli, M
    Cascarano, GL
    Giacovazzo, C
    Guagliardi, A
    Moliterni, AGG
    Polidori, G
    Spagna, R
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1999, 32 : 115 - 119
  • [3] Tautomerism of azacycles:: III.: Molecular and crystal structures of 3H- and 2-phenyl-1H,4H-4,5-dihydro-1,2,4-triazole-5-thiones
    Buzykin, B. I.
    Mironova, E. V.
    Gubaidullin, A. T.
    Litvinov, I. A.
    Nabiullin, V. N.
    [J]. RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2008, 78 (04) : 634 - 648
  • [4] Tri-substituted triazoles as potent non-nucleoside inhibitors of the HIV-1 reverse transcriptase
    De La Rosa, Martha
    Kim, Hong Woo
    Gunic, Esmir
    Jenket, Cheryl
    Boyle, Uyen
    Koh, Yung-hyo
    Korboukh, Ilia
    Allan, Matthew
    Zhang, Weijian
    Chen, Huanming
    Xu, Wen
    Nilar, Shahul
    Yao, Nanhua
    Hamatake, Robert
    Lang, Stanley A.
    Hong, Zhi
    Zhang, Zhijun
    Girardet, Jean-Luc
    [J]. BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 2006, 16 (17) : 4444 - 4449
  • [5] N-Carbethoxy-N′-[3-(4-methylphenyl)-1H-1,2,4-triazol-5-yl]thiourea
    Dolzhenko, Anton V.
    Tan, Geok Kheng
    Koh, Lip Lin
    Dolzhenko, Anna V.
    Chui, Wai Keung
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O549 - U4426
  • [6] Farrugia L. J. J., 1999, Appl. Crystallogr, V32, P837, DOI [10.1107/S0021889812029111, DOI 10.1107/S0021889812029111, 10.1107/S0021889899006020.35E.M.]
  • [7] ON ENANTIOMORPH-POLARITY ESTIMATION
    FLACK, HD
    [J]. ACTA CRYSTALLOGRAPHICA SECTION A, 1983, 39 (NOV): : 876 - 881
  • [8] X-ray crystallographic and theoretical study of 4-cyclohexyl-5-(2-furyl)-2,4-dihydro-3H-1,2,4-triazole-3-thione
    Karayel, Arzu
    Oezbey, Sueheyla
    Capan, Gueltaze
    [J]. JOURNAL OF MOLECULAR STRUCTURE, 2007, 841 (1-3) : 118 - 124
  • [9] Synthesis, cytotoxicity and effects of some 1,2,4-triazole and 1,3,4-thiadiazole derivatives on immunocompetent cells
    Mavrova, Anelia Ts.
    Wesselinova, Diana
    Tsenov, Yordan A.
    Denkova, Pavletta
    [J]. EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2009, 44 (01) : 63 - 69
  • [10] A short history of SHELX
    Sheldrick, George M.
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122