Study of the structural and magnetic properties of Pd-substituted CoFe2O4 materials obtained by a fast method

被引:5
|
作者
Vlazan, Paulina [1 ]
Poienar, Maria [1 ]
Rus, Florina Stefania [1 ]
Sfirloaga, Paula [1 ]
机构
[1] Natl Inst Res & Dev Electrochem & Condensed Matte, Dr AP Podeanu St 144, Timisoara 300569, Romania
关键词
Fast method; Cobalt ferrite nanomaterials; X-Ray diffraction; Magnetic properties; COBALT FERRITE; MAGNETOCRYSTALLINE ANISOTROPY; NANOPARTICLES; MICROSTRUCTURE; MAGNESIUM;
D O I
10.1016/j.physb.2021.413073
中图分类号
O469 [凝聚态物理学];
学科分类号
070205 ;
摘要
An efficient fast hydrothermal method was used to synthesize Co1-xPdxFe2O4 (x = 0, 0.05, 0.1 and 0.5) nanocrystalline powders, where Co2+ was substituted with Pd2+ ions. The materials crystallize within the spinel structure (Fd-3m) with crystallites sizes varying between 5.6 and 17.6 nm. The particles present a cubic shape for x = 0 and x = 0.1 samples and the presence of Pd in samples was confirmed by Energy-dispersive X-Ray spectroscopy (EDX) analysis. The magnetic hysteresis loops indicate that the saturation magnetization decreases with the increase once with of the Pd2+ amount substitution (from -52 emu/g for x = 0--7 emu/g for x = 0.5).
引用
收藏
页数:6
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