The fabrication of SiBCN ceramic components from preceramic polymers by digital light processing (DLP) 3D printing technology

被引：121

作者：

Li, Shan ^{[1
]}

Duan, Wenyan ^{[1
]}

Zhao, Tong ^{[3
]}

Han, Weijian ^{[3
]}

Wang, Li ^{[1
]}

Dou, Rui ^{[1
]}

Wang, Gong ^{[1
,2
]}

机构：

[1] Chinese Acad Sci, Key Lab Space Mfg Technol SMT, Beijing 100094, Peoples R China

[2] Univ Chinese Acad Sci, Beijing 100049, Peoples R China

[3] Chinese Acad Sci, Inst Chem, Lab Adv Polymer Mat, Beijing 100190, Peoples R China

来源：

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY | 2018年 / 38卷 / 14期

关键词：

SiBCN ceramic components; 3D printing; Photocurable; Polyborosilazane; SINGLE-SOURCE-PRECURSOR; C-N CERAMICS; STEREOLITHOGRAPHY; PHOTOPOLYMERIZATION; FIBERS; CRYSTALLIZATION;

D O I：

10.1016/j.jeurceramsoc.2018.06.046

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

We present a novel method to fabricate SiBCN ceramic components with complex shapes from preceramic polymers by using digital light processing (DLP) 3D printing technology in this research work. The photocurable precursor for 3D printing was prepared by blending high ceramic yield polyborosilazane with photosensitive acrylate monomers. The material formulation and printing parameters were optimized to fabricate complicated SiBCN ceramic components with high precision. The printed SiBCN ceramic materials were pyrolyzed at different temperatures, and retained their fine features after pyrolysis. Their microstructures were characterized by FTIR, XRD and TEM respectively. Furthermore, the thermal stability and mechanical properties of the SiBCN ceramic samples were investigated and discussed in detail. The 3D printed SiBCN ceramic material exhibited excellent thermal stability and resistance to high temperature oxidation up to 1500 degrees C.

引用

页码：4597 / 4603

页数：7

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