Investigation of Factors Affecting Synthesis of Polyvinyl Butyral by Taguchi Method

被引：28

作者：

Hajian, Morteza ^{[1
]}

Koohmareh, Gholam Ali ^{[1
]}

Rastgoo, Mahdi ^{[1
]}

机构：

[1] Univ Isfahan, Fac Sci, Dept Chem, Esfahan 8174673441, Iran

来源：

JOURNAL OF APPLIED POLYMER SCIENCE | 2010年 / 115卷 / 06期

关键词：

modification; polycondensation; synthesis; thermogravimetric analysis (TGA); MISCIBILITY;

D O I：

10.1002/app.30603

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

Polyvinyl butyral (PVB) was prepared by condensation reaction of butyral with polyvinyl alcohol (PVA) in aqueous phase containing an acid as a catalyst and an emulsifying agent. Properties of the polymer were a function of the relative amounts of the three randomly distributed units of acetal, acetate and vinyl alcohol groups, and the molecular weight. In this work, some effective factors in synthesis of PVB have been investigated by Taguchi method. The percent of the acetalization has been determined according to the ASTM D1396, and the polymer was characterized by IR, TG, and DTG techniques. (C) 2009 Wiley Periodicals, Inc. J Appl Polym Sci 115: 3592-3597, 2010

引用

页码：3592 / 3597

页数：6

共 12 条

[1] The characterization of polyvinyl butyral by thermal analysis [J].

Dhaliwal, AK ;

Hay, JN .

THERMOCHIMICA ACTA, 2002, 391 (1-2) :245-255

[2] Miscibility of polyvinyl butyral/nylon 6 blends [J].

Jeong, HK ;

Rooney, M ;

David, DJ ;

MacKnight, WJ ;

Karasz, FE ;

Kajiyama, T .

POLYMER, 2000, 41 (15) :6003-6013

[3]

LAVIN E, 1950, Patent No. 2496480

[4] Degradation of poly(vinyl butyral) and its stabilization by bases [J].

Liu, Rong ;

He, Bobing ;

Chen, Xian .

POLYMER DEGRADATION AND STABILITY, 2008, 93 (04) :846-853

[5]

PENFOLD AR, 1956, PLASTICS SYNTHETIC F

[6]

ROBERT D, 1987, Patent No. 4652320

[7]

ROBERT D, 1994, Patent No. 5349014

[8]

ROMBACH LH, 1964, Patent No. 3153009

[9]

STAMATOFF GS, 1947, Patent No. 2422754

[10]

STAMATOFF GS, 1946, Patent No. 2400957

← 1 2 →