Fabrication of freestanding 2"-GaN wafers by hydride vapour phase epitaxy and self-separation during cooldown

被引:28
作者
Lipski, Frank [1 ]
Wunderer, Thomas [1 ]
Schwaiger, Stephan [1 ]
Scholz, Ferdinand [1 ]
机构
[1] Univ Ulm, Inst Optoelect, Ulm, Germany
来源
PHYSICA STATUS SOLIDI A-APPLICATIONS AND MATERIALS SCIENCE | 2010年 / 207卷 / 06期
关键词
GaN; morphology; patterning; structure; VPE; PROCESS OPTIMIZATION; GAN LAYERS; GROWTH; HVPE;
D O I
10.1002/pssa.200983517
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Using a dielectric mask, structured by optical lithography, freestanding 2 ''-GaN wafers were prepared by hydride vapour phase epitaxy (HVPE) and self-separation during cooldown. The mask was deposited on a GaN template grown on sapphire by metal organic vapour phase epitaxy (MOVPE) and it was shown that the instability of a SiN mask at growth temperature supports the further self-separation. Testing different mask geometries, a hexagonally shaped pattern with a period of 30 mu m and an opening of 3 mu m showed best performance. This mask allowed the growth and separation of a full 2 '' GaN wafer by utilizing the stress arising during cooldown from thermal mismatch to the substrate. Thickness inhomogenity was below 10% and the samples show good surface morphology. (C) 2010 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
引用
收藏
页码:1287 / 1291
页数:5
相关论文
共 10 条
[1]   HVPE growth of high quality GaN layers [J].
Brueckner, Peter ;
Habel, Frank ;
Scholz, Ferdinand .
PHYSICA STATUS SOLIDI C - CURRENT TOPICS IN SOLID STATE PHYSICS, VOL 3, NO 6, 2006, 3 (06) :1471-1474
[2]   Determination of dislocation density in epitaxially grown GaN using an HCl etching process [J].
Habel, F ;
Seyboth, M .
5TH INTERNATIONAL CONFERENCE ON NITRIDE SEMICONDUCTORS (ICNS-5), PROCEEDINGS, 2003, 0 (07) :2448-2451
[3]   Self-separation of thick two inch GaN layers grown by HVPE on sapphire using epitaxial lateral overgrowth with masks containing tungsten [J].
Hennig, Ch. ;
Richter, E. ;
Weyers, M. ;
Traenkle, G. .
PHYSICA STATUS SOLIDI C - CURRENT TOPICS IN SOLID STATE PHYSICS, VOL 4 NO 7 2007, 2007, 4 (07) :2638-+
[4]   Process optimization for the effective reduction of threading dislocations in MOVPE grown GaN using in situ deposited SiNx masks [J].
Hertkorn, J. ;
Lipski, F. ;
Brueckner, R. ;
Wunderer, T. ;
Thapa, S. B. ;
Scholz, F. ;
Chuvilin, A. ;
Kaiser, U. ;
Beer, M. ;
Zweck, J. .
JOURNAL OF CRYSTAL GROWTH, 2008, 310 (23) :4867-4870
[5]   Studies towards freestanding GaN in hydride vapor phase epitaxy by in-situ etching of a sacrificial ZnO buffer layer [J].
Lipski, Frank ;
Thapa, Sarad B. ;
Hertkorn, Joachim ;
Wunderer, Thomas ;
Schwaiger, Stephan ;
Scholz, Ferdinand ;
Feneberg, Martin ;
Wiedenmann, Michael ;
Thonke, Klaus ;
Hochmuth, Holger ;
Lorenz, Michael ;
Grundmann, Marius .
PHYSICA STATUS SOLIDI C: CURRENT TOPICS IN SOLID STATE PHYSICS, VOL 6, SUPPL 2, 2009, 6 :S352-S355
[6]  
Miskys CR, 2003, GROUP III-NITRIDES AND THEIR HETEROSTRUCTURES: GROWTH, CHARACTERIZATION AND APPLICATIONS, P1627, DOI 10.1002/pssc.200303140
[7]   Preparation of large freestanding GaN substrates by hydride vapor phase epitaxy using GaAs as a starting substrate [J].
Motoki, K ;
Okahisa, T ;
Matsumoto, N ;
Matsushima, M ;
Kimura, H ;
Kasai, H ;
Takemoto, K ;
Uematsu, K ;
Hirano, T ;
Nakayama, M ;
Nakahata, S ;
Ueno, M ;
Hara, D ;
Kumagai, Y ;
Koukitu, A ;
Seki, H .
JAPANESE JOURNAL OF APPLIED PHYSICS PART 2-LETTERS & EXPRESS LETTERS, 2001, 40 (2B) :L140-L143
[8]   InGaN/GaN/AlGaN-based laser diodes with cleaved facets grown on GaN substrates [J].
Nakamura, S ;
Senoh, M ;
Nagahama, S ;
Iwasa, N ;
Yamada, T ;
Matsushita, T ;
Kiyoku, H ;
Sugimoto, Y ;
Kozaki, T ;
Umemoto, H ;
Sano, M ;
Chocho, K .
APPLIED PHYSICS LETTERS, 1998, 73 (06) :832-834
[9]   Reactor and growth process optimization for growth of thick GaN layers on sapphire substrates by HVPE [J].
Richter, E ;
Hennig, C ;
Weyers, M ;
Habel, F ;
Tsay, JD ;
Liu, WY ;
Brückner, P ;
Scholz, F ;
Makarov, Y ;
Segal, A ;
Kaeppeler, J .
JOURNAL OF CRYSTAL GROWTH, 2005, 277 (1-4) :6-12
[10]   Bulk gallium nitride: preparation and study of properties [J].
Zhilyaev, YV ;
Nasonov, AV ;
Raevski, SD ;
Rodin, SN ;
Shcheglov, MP ;
Davydov, VY .
PHYSICA STATUS SOLIDI A-APPLICATIONS AND MATERIALS SCIENCE, 2003, 195 (01) :122-126