Solid phase extraction of uranium(VI) on phosphorus-containing polymer grafted 4-aminoantipyrine

被引：17

作者：

Soylak, Mustafa ^{[1
]}

Khan, Mansoor ^{[1
,2
]}

Alosmanov, Rasim ^{[3
]}

Shah, Jasmin ^{[2
]}

Jan, Mohammad Rasul ^{[2
]}

机构：

[1] Erciyes Univ, Dept Chem, Fac Sci, TR-38039 Kayseri, Turkey

[2] Univ Peshawar, Inst Chem Sci, Peshawar, Pakistan

[3] Baku State Univ, Dept Chem, Z Khalilov Str 23, AZ-1148 Baku, Azerbaijan

来源：

JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY | 2016年 / 308卷 / 03期

关键词：

Solid phase extraction; Spectrophotometry; Determination; Uranium; Arsenazo(III); MULTIWALLED CARBON NANOTUBES; AQUEOUS-SOLUTIONS; ACTIVATED CARBON; WATER SAMPLES; SPECTROPHOTOMETRIC DETERMINATION; CHITOSAN RESIN; TRACE LEVELS; METAL-IONS; PRECONCENTRATION; SEPARATION;

D O I：

10.1007/s10967-015-4508-4

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Phosphorus-containing polymer grafted 4-aminoantipyrine has been synthesized and used for solid phase extraction of U(VI) prior to its UV-Visible spectrophotometric determination by using arsenazo(III). The adsorbent was characterized by using FT-IR and SEM analysis. The influence of parameters including pH, adsorbent dose, amount of complexing reagent, sample volume and matrix effect have been optimized. The detection limit was determined as 1.4 mu g L-1 with pre-concentration factor of 30 and RSD of 1.4 %. The accuracy was checked by the analysis of GBW07424 soil and TMDA-64.2 environmental water certified reference materials. The method was applied to natural water and soil samples.

引用

页码：955 / 963

页数：9

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