Electrosynthesis of a bis-ketenedithioacetal disulphide derivative from 1-phenyl-3-methyl-4-butyldithiocarboxylate-5-pyrazolone using a glassy carbon electrode

被引：1

作者：

Oliva, A ^{[1
]}

Molinari, A ^{[1
]}

Angulo, J ^{[1
]}

Schrebler, R ^{[1
]}

Gómez, H ^{[1
]}

Córdova, R ^{[1
]}

机构：

[1] Pontificia Univ Catolica Valparaiso, Inst Quim, Valparaiso, Chile

来源：

SYNTHETIC COMMUNICATIONS | 2000年 / 30卷 / 23期

关键词：

D O I：

10.1080/00397910008087058

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The electrooxidation of 1-phenyl-3-methyl-4-butyldithiocarboxylate- 5-pyrazolone 1 has been studied in ethanol/water solution, using a glassy carbon electrode surface. The electrochemical and spectroscopic data are in agreement with a bis-ketenedithioacetal disulphide compound 2 as the only product of the reaction.

引用

页码：4353 / 4360

页数：8

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