X-ray nanotomography characterizations of gold foams

被引:2
作者
Li, Zhaoguo [1 ]
Luo, Jiangshan [1 ]
Tan, Xiulan [1 ]
Fang, Qi [1 ]
Zeng, Yong [1 ]
Zhou, Minjie [1 ]
Wu, Weidong [1 ]
Zhang, Jicheng [1 ]
机构
[1] China Acad Engn Phys, Res Ctr Laser Fus, Mianyang 621900, Peoples R China
基金
中国国家自然科学基金;
关键词
X-ray nanotomography; Gold foams; Microstructures; Structure characterization; TOMOGRAPHY;
D O I
10.1016/j.matlet.2017.06.056
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Observation of the three-dimensional interior microstructure of low-density gold foams is very important for the optimization of their physical and chemical properties. We report on the threedimensional internal microstructural imaging of gold foams by using X-ray computed tomography with a resolution of 50 nm. The gold foams are synthesized by the chemical dealloying method. By using focused ion beam milling technology, a foam micro-cylinder with a diameter of approximately 55 lm is prepared. The tomographical data sets of the micro-cylinder foam are collected in the angle range of +/-degrees 90 at a photon energy of 8 keV. The data sets are then used to reconstruct the three-dimensional microstructure of the gold foams. The three-dimensional reconstruction information obtained from computed tomography provides an intuitive understanding of the gold foam structure. (C) 2017 Published by Elsevier B.V.
引用
收藏
页码:215 / 218
页数:4
相关论文
共 18 条
[1]   Nanoporous plasmonic metamaterials [J].
Biener, Juergen ;
Nyce, Gregory W. ;
Hodge, Andrea M. ;
Biener, Monika M. ;
Hamza, Alex V. ;
Maier, Stefan A. .
ADVANCED MATERIALS, 2008, 20 (06) :1211-1217
[2]   Soft X-ray microscopy at a spatial resolution better than 15nm [J].
Chao, WL ;
Harteneck, BD ;
Liddle, JA ;
Anderson, EH ;
Attwood, DT .
NATURE, 2005, 435 (7046) :1210-1213
[3]   Three-dimensional imaging of a complex concaved cuboctahedron copper sulfide crystal by x-ray nanotomography [J].
Chen, Jie ;
Wu, Chunyan ;
Tian, Jinping ;
Li, Wenjie ;
Yu, Shuhong ;
Tian, Yangchao .
APPLIED PHYSICS LETTERS, 2008, 92 (23)
[4]   Morphological and topological analysis of coarsened nanoporous gold by x-ray nanotomography [J].
Chen, Yu-chen Karen ;
Chu, Yong S. ;
Yi, JaeMock ;
McNulty, Ian ;
Shen, Qun ;
Voorhees, Peter W. ;
Dunand, David C. .
APPLIED PHYSICS LETTERS, 2010, 96 (04)
[5]   Hard-x-ray microscopy with Fresnel zone plates reaches 40 nm Rayleigh resolution [J].
Chu, Y. S. ;
Yi, J. M. ;
De Carlo, F. ;
Shen, Q. ;
Lee, Wah-Keat ;
Wu, H. J. ;
Wang, C. L. ;
Wang, J. Y. ;
Liu, C. J. ;
Wang, C. H. ;
Wu, S. R. ;
Chien, C. C. ;
Hwu, Y. ;
Tkachuk, A. ;
Yun, W. ;
Feser, M. ;
Liang, K. S. ;
Yang, C. S. ;
Je, J. H. ;
Margaritondo, G. .
APPLIED PHYSICS LETTERS, 2008, 92 (10)
[6]   Nanoporous Metals for Catalytic and Optical Applications [J].
Ding, Yi ;
Chen, Mingwei .
MRS BULLETIN, 2009, 34 (08) :569-576
[7]   Element-Specific X-Ray Phase Tomography of 3D Structures at the Nanoscale [J].
Donnelly, Claire ;
Guizar-Sicairos, Manuel ;
Scagnoli, Valerio ;
Holler, Mirko ;
Huthwelker, Thomas ;
Menzel, Andreas ;
Vartiainen, Ismo ;
Mueller, Elisabeth ;
Kirk, Eugenie ;
Gliga, Sebastian ;
Raabe, Joerg ;
Heyderman, Laura J. .
PHYSICAL REVIEW LETTERS, 2015, 114 (11)
[8]   Three-dimensional morphology of nanoporous gold [J].
Fujita, Takeshi ;
Qian, Li-Hua ;
Inoke, Koji ;
Erlebacher, Jonah ;
Chen, Ming-Wei .
APPLIED PHYSICS LETTERS, 2008, 92 (25)
[9]   Revealing the micromechanisms behind semi-solid metal deformation with time-resolved X-ray tomography [J].
Kareh, K. M. ;
Lee, P. D. ;
Atwood, R. C. ;
Connolley, T. ;
Gourlay, C. M. .
NATURE COMMUNICATIONS, 2014, 5
[10]   Quantitative study of interior nanostructure in hollow zinc oxide particles on the basis of nondestructive x-ray nanotomography [J].
Li, Wenjie ;
Wang, Ning ;
Chen, Jie ;
Liu, Gang ;
Pan, Zhiyun ;
Guan, Yong ;
Yang, Yunhao ;
Wu, Wenquan ;
Tian, Jinping ;
Wei, Shiqiang ;
Wu, Ziyu ;
Tian, Yangchao ;
Guo, Lin .
APPLIED PHYSICS LETTERS, 2009, 95 (05)