Determination of p-Phenylenediamine Using Electrochemically Reduced Graphene Oxide

被引:0
作者
Wang, Chunyan [1 ]
Lan, Yanfei [1 ]
Liao, Binqian [1 ]
Li, Dan [1 ]
Zhu, Meiwu [1 ]
机构
[1] E China Inst Technol, Dept Mat Sci & Engn, Fundamental Sci Radioact Geol & Explorat Technol, Fuzhou 344000, Peoples R China
基金
中国国家自然科学基金;
关键词
Determination; p-Phenylenediamine; Electrochemically reduced graphene oxide; LARGE-AREA; FILMS; SHEETS;
D O I
10.14233/ajchem.2014.16643
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In this communication, we report a green and effective approach to construct a sensitive detection platform based on electrochemically reduced graphene oxide modified electrode (EG@GCE). The surface morphology and structure of electrochemical reduction of graphene oxide were investigated by utilizing transmission electron microscope, FT-IR spectra, UV-visible spectra and X-ray diffraction. This EG@GCE exhibits sensitive current responses toward the electrooxidation of p-phenylenediamine (PDA) due to the excellent conductivity and large electroactive surface area of electrochemical reduction of graphene oxide and the strong p-p stacking interactions between p-phenylenediamine and the electrochemical reduction of graphene oxide surface. Moreover, a low detection limit of 1.08 mu M (S/N = 3) with the linear range of 5 to 200 mu M is obtained. This new finding demonstrates that the electrochemical reduction of graphene oxide is a promising candidate of advanced electrode materials for electrochemical determination aromatic amines in environmental analysis.
引用
收藏
页码:4381 / 4385
页数:5
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