Response surface optimization of SPME extraction conditions for the analysis of volatile compounds in Brazilian sugar cane spirits by HS-SPME-GC-MS

被引：14

作者：

Zacaroni, Lidiany Mendonca ^{[1
]}

de Sales, Priscila Ferreira ^{[1
]}

Cardoso, Maria das Gracas ^{[1
]}

Santiago, Wilder Douglas ^{[1
]}

Nelson, David Lee ^{[2
]}

机构：

[1] Univ Fed Lavras, Dept Chem, Univ Campus,CP 3037, BR-37200000 Lavras, MG, Brazil

[2] Fed Univ Jequitinhonha & Mucuri Valleys, Res & Grad Program, Diamantina, MG, Brazil

来源：

JOURNAL OF THE INSTITUTE OF BREWING | 2017年 / 123卷 / 02期

关键词：

volatile compounds; distilled sugarcane spirits; solid-phase microextraction; response surface method; SOLID-PHASE MICROEXTRACTION;

D O I：

10.1002/jib.410

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

The extraction of volatile compounds from distilled sugarcane spirits was investigated using central composite design associated with response surface methodology. The parameters evaluated were the extraction temperature, extraction time and desorption time. All of the parameters analysed, as well as their interactions, were significant for the process at a 95% confidence level. Although the extraction time and extraction temperature exhibited positive effects, the desorption time showed a negative effect. The second-order polynomial model was adjusted appropriately for the response surface analysis. The optimized conditions were extraction temperature equal to 45 degrees C, extraction time of 50 min and the desorption time corresponding to 100 s. (C) 2017 The Institute of Brewing & Distilling

引用

页码：226 / 231

页数：6

共 26 条

[1] Chemometric approach to the optimization of HS-SPME/GC-MS for the determination of multiclass pesticide residues in fruits and vegetables [J].

Abdulra'uf, Lukman Bola ;

Tan, Guan Huat .

FOOD CHEMISTRY, 2015, 177 :267-273

[2]

Adams R.P., 2007, IDENTIFICATION ESSEN, V4th

[3]

Alpendurada MD, 2000, J CHROMATOGR A, V889, P3

[4]

Barbetta PA, 2000, QUAL RELIAB ENG INT, V16, P397, DOI 10.1002/1099-1638(200009/10)16:5<397::AID-QRE348>3.0.CO

[5]

2-X

[6] Congeners in sugar cane spirits aged in casks of different woods [J].

Bortoletto, Aline M. ;

Alcarde, Andre R. .

FOOD CHEMISTRY, 2013, 139 (1-4) :695-701

[7]

Box G. E., 1978, Statistics for experimenters, V664

[8]

Brasil, 2005, PECUARIA ABASTECIMEN

[9] Development and validation of method for heterocyclic compounds in wine: Optimization of HS-SPME conditions applying a response surface methodology [J].

Burin, Vivian Maria ;

Marchand, Stephanie ;

de Revel, Gilles ;

Bordignon-Luiz, Marilde T. .

TALANTA, 2013, 117 :87-93

[10]

Cancado Junior F. L., 2009, Informe Agropecuario, V30, P7

← 1 2 3 →