Comparison of different methods for characterizing multi-walled carbon nanotubes

被引：23
作者：
Gommes, C
Blacher, S
Dupont-Pavlovsky, N
Bossuot, C
Lamy, M
Brasseur, A
Marguillier, D
Fonseca, A
McRae, E
Nagy, JB
Pirard, JP
机构：
[1] Univ Liege, Lab Genie Chim, B-4000 Liege, Belgium
[2] Univ Henri Poincare Nancy, UMR 7555, Lab Chim Solide Mineral, F-54506 Vandoeuvre Les Nancy, France
[3] Fac Univ Notre Dame Paix, Lab Resonance Magnet Nucl, B-5000 Namur, Belgium
[4] Univ Liege, Lab Chim Inorgan Struct, B-4000 Liege, Belgium
来源：
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS | 2004年 / 241卷 / 1-3期
关键词：
carbon nanotubes; image analysis; gas adsorption; X-ray scattering; thermogravimetry;
D O I：
10.1016/j.colsurfa.2004.04.050
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Four complementary and independent methods are used to characterize nanotube samples: (i) TEM observation coupled with image analysis, (ii) nitrogen and krypton adsorption isotherm analysis, (iii) thermogravimetry and (iv) wide angle X-ray scattering. The methodology is discussed on the basis of two multi-walled carbon nanotube samples produced by the CCVD technique with very different reaction rates. It is shown that the total amount of deposited carbon is larger for the sample produced at the higher rate, that the fraction of nanotubes in the deposited carbon does not seem to be significantly different, but that the crystallinity of the nanotubes wall is larger for the sample produced at the lowest reaction rate. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码：155 / 164
页数：10
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