Flux Assisted Shape Tunable Synthesis of Zinc Oxide Microflowers

被引：4
|
作者：
Amutha, R. [1 ]
Muruganandham, M. [1 ]
Lee, G. J. [1 ]
Batalova, V. N. [2 ]
Mokrousov, G. [2 ]
Wu, J. J. [1 ]
机构：
[1] Feng Chia Univ, Dept Environm Engn & Sci, Taichung 40704, Taiwan
[2] Tomsk State Univ, Dept Analyt Chem, Tomsk, Russia
来源：
ADVANCED SCIENCE LETTERS | 2010年 / 3卷 / 04期
关键词：
ZNO NANORODS; OPTICAL-PROPERTIES; GROWTH; NANOSTRUCTURES; NANOWIRES; FILMS;
D O I：
10.1166/asl.2010.1165
中图分类号：
O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];
学科分类号：
07 ; 0710 ; 09 ;
摘要：
A simple template free ZnO microflowers have been successfully fabricated by using a simple thermal decomposition process. Thermal decomposition of zinc acetate facilitated at 205 C for 12 h results flower shaped ZnO. The microflowers were self-assembled by microrods. The effect of addition of NaCl flux on the morphology and crystal structure has been investigated and the results indicated that the addition of flux influenced the morphology of the synthesized ZnO. The XRD results indicated formation of pure wurtzite phase ZnO at both conditions and HR-TEM results confirmed single and polycrystalline nature of ZnO in the absence and presence of flux respectively. A plausible mechanism of microflower has been discussed on the basis of experimental results.
引用
收藏
页码：491 / 495
页数：5
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