Online Process Analytics with XRF and LIBS for the Control of the Recycling of Sewage Sludge Ashes

被引:2
作者
Ostermann, Markus [1 ]
Herzel, Hannes [1 ]
Kuehn, Andreas [2 ]
Wedell, Reiner [2 ]
Mory, David [3 ]
机构
[1] Bundesanstalt Mat Forsch & Prufung BAM, Unter Eichen 87, D-12205 Berlin, Germany
[2] IAP Inst Angew Photon eV, Rudower Chaussee 29-31, D-12489 Berlin, Germany
[3] LTB Lasertech Berlin GmbH, Studio 2c, D-12489 Berlin, Germany
关键词
Laser-induced breakdown spectroscopy; Phosphorus; Process analysis; Sewage sludge ash; X-ray fluorescence spectroscopy; LASER; STEEL; IDENTIFICATION;
D O I
10.1002/cite.201500186
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Resources from sewage sludge ashes can be re-utilized for the recycling economy and pollutants can be removed by using a thermochemical process. An online analysis method has been developed for the determination of element mass fractions in the ashes and their products originating from the process. The applied analysis system is a method combination of laser-induced breakdown spectroscopy (LIBS) and X-ray fluorescence (XRF) spectroscopy. Robustness and a modular construction are important demands for successful future applications.
引用
收藏
页码:786 / 792
页数:7
相关论文
共 16 条
[1]  
Adam C., 2009, RESULTS EUROPEAN FP6
[2]  
[Anonymous], 2006, Handbook of Laser-Induced Breakdown Spectroscopy
[3]  
Beckhoff B., 2006, HDB PRACTICAL XRAY F, VXIX
[4]   Process analysis of recycled thermoplasts from consumer electronics by laser-induced plasma spectroscopy [J].
Fink, H ;
Panne, U ;
Niessner, R .
ANALYTICAL CHEMISTRY, 2002, 74 (17) :4334-4342
[5]   Identification of solid materials by correlation analysis using a microscopic laser-induced plasma spectrometer [J].
Gornushkin, IB ;
Smith, BW ;
Nasajpour, H ;
Winefordner, JD .
ANALYTICAL CHEMISTRY, 1999, 71 (22) :5157-5164
[6]   Identification of particulate materials by correlation analysis using a microscopic laser induced breakdown spectrometer [J].
Gornushkin, IB ;
Ruíz-Medina, A ;
Anzano, JM ;
Smith, BW ;
Winefordner, JD .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 2000, 15 (06) :581-586
[7]   Determination of cobalt in soil, steel, and graphite using excited-state laser fluorescence induced in a laser spark [J].
Gornushkin, IB ;
Kim, JE ;
Smith, BW ;
Baker, SA .
APPLIED SPECTROSCOPY, 1997, 51 (07) :1055-1059
[8]   Rapid in-situ analysis of liquid steel by laser-induced breakdown spectroscopy [J].
Gruber, J ;
Heitz, J ;
Strasser, H ;
Bäuerle, D ;
Ramaseder, N .
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 2001, 56 (06) :685-693
[9]   Sewage sludge ash - A promising secondary phosphorus source for fertilizer production [J].
Herzel, Hannes ;
Krueger, Oliver ;
Hermann, Ludwig ;
Adam, Christian .
SCIENCE OF THE TOTAL ENVIRONMENT, 2016, 542 :1136-1143
[10]   Recovery potential of German sewage sludge ash [J].
Krueger, Oliver ;
Adam, Christian .
WASTE MANAGEMENT, 2015, 45 :400-406