Growth and properties of ytterbium doped KY(WO4)2 nanocomposites

被引:3
作者
Borowiec, M. T. [1 ]
Deptula, A. [2 ]
Lojkowski, W. [3 ]
Gierlotka, S. [3 ]
Dyakonov, V. P. [1 ]
Lada, W. [2 ]
Olczak, T. [2 ]
Wawszczak, D. [2 ]
Aleshkevych, P. [1 ]
Domuchowski, W. [1 ]
Zayarnyuk, T. [1 ]
Baranski, M. [1 ]
Czech, M. [1 ]
Szymczak, H. [1 ]
机构
[1] Polish Acad Sci, Inst Phys, Al Lotnikow 32-46, PL-02668 Warsaw, Poland
[2] Inst Nuclear Chem & Technol, PL-03175 Warsaw, Poland
[3] Polish Acad Sci, Inst High Pressure Phys, PL-01142 Warsaw, Poland
来源
DOPED NANOPOWDERS: SYNTHESIS, CHARACTERISATION APPLICATIONS | 2007年 / 128卷
关键词
Complex Sol-Gel Process; nanocrystals of KY(WO4)(2) and KY(WO4)(2)+1 % mol Yb;
D O I
10.4028/www.scientific.net/SSP.128.25
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Nanocomposites (nanocrystals) of KY(WO4)(2) and KY(WO4)(2)+1% Mol Yb were synthesized using a Complex Sol-Gel Process (CSGP). A chemical treatment with concentrated nitric acid and hydrogen peroxide was used to reduce the clecarbonisation temperature. The expected monoclinic phase C2/c of the KYW of the nanocomposite powder was confirmed using XDR. Front the X-ray diffraction measurements, the unit cell parameters and the size of nanoparticles was determined. Electron spin resonance studies in the X band were carried out on KYW and KYW:Yb nanocrystals. The sintered samples were made with using the high pressure technique at temperatures up to 600 degrees C. In addition chemical analysis, X-ray diffraction measurements and ESR investigations were carried out on the sintered samples.
引用
收藏
页码:25 / +
页数:2
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