Preparation of silicon carbide using bamboo charcoal as carbon source

被引:19
作者
Xingzhong, Guo [1 ]
Lingjie, Zhang [1 ]
Liqing, Yan [1 ]
Hui, Yang [1 ]
Lin, Zhu [1 ]
机构
[1] Zhejiang Univ, Dept Mat Sci & Engn, Hangzhou 310027, Peoples R China
关键词
Silicon carbide; XRD; SEM; COMBUSTION SYNTHESIS;
D O I
10.1016/j.matlet.2009.11.006
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Silicon carbide (SiC) was prepared by carbothermal reduction with amorphous silica sol as silicon source and bamboo charcoal powder as carbon source. The compositions and microstructure of prepared SiC were investigated by using X-ray diffraction (XRD), scanning electron microscopy (SEM) and Energy Dispersive X-ray Spectroscopy (EDS). XRD of prepared SiC showed that the major phase of prepared SiC was hexagonal 6H-SiC with the existence of some 4H-SiC. SEM showed that SiC particle was granular, rod-like and of tower-shape, and it inherited the shape of bamboo charcoal. EDS showed that prepared SiC was pure without being doped by the mineral elements from bamboo charcoal. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:331 / 333
页数:3
相关论文
共 10 条
  • [1] DISHUN Z, 2008, APPL SURF SCI, V254, P3242
  • [2] Microwave hybrid synthesis of silicon carbide nanopowders
    Ebadzadeh, Touradj
    Marzban-Rad, Ehsan
    [J]. MATERIALS CHARACTERIZATION, 2009, 60 (01) : 69 - 72
  • [3] JIALU D, 2007, J MAT SCI ENG, V25, P743
  • [4] JIANGTAO Z, 2009, CARBON, V47, P1614
  • [5] SOLID COMBUSTION SYNTHESIS OF BETA-SIC POWDERS
    PAMPUCH, R
    STOBIERSKI, L
    LIS, J
    RACZKA, M
    [J]. MATERIALS RESEARCH BULLETIN, 1987, 22 (09) : 1225 - 1231
  • [6] Microwave initiated self-propagating high-temperature synthesis of SiC
    Peng, JH
    Binner, J
    Bradshaw, S
    [J]. JOURNAL OF MATERIALS SYNTHESIS AND PROCESSING, 2001, 9 (06) : 363 - 368
  • [7] SEON WS, 2000, J AM CERAM SOC, V83, P2584
  • [8] KINETICS OF CARBOTHERMAL REDUCTION SYNTHESIS OF BETA SILICON-CARBIDE
    WEIMER, AW
    NILSEN, KJ
    COCHRAN, GA
    ROACH, RP
    [J]. AICHE JOURNAL, 1993, 39 (03) : 493 - 503
  • [9] Synthesis of SiC by silicon and carbon combustion in air
    Yang, Yun
    Lin, Zhi-Ming
    Li, Jiang-Tao
    [J]. JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2009, 29 (01) : 175 - 180
  • [10] Mechanical-activation-assisted combustion synthesis of SiC
    Yang, Yun
    Yang, Kun
    Lin, Zhi-Ming
    Li, Jiang-Tao
    [J]. MATERIALS LETTERS, 2007, 61 (03) : 671 - 676