Performance and first results of the ELETTRA high-flux beamline for small-angle X-ray scattering

被引:124
作者
Amenitsch, H
Bernstorff, S
Kriechbaum, M
Lombardo, D
Mio, H
Rappolt, M
Laggner, P
机构
[1] Austrian Acad Sci, Inst Biophys & Xray Struct Res, A-8010 Graz, Austria
[2] Sincrotrone Trieste, I-34012 Trieste, Italy
来源
JOURNAL OF APPLIED CRYSTALLOGRAPHY | 1997年 / 30卷 / 02期
关键词
D O I
10.1107/S0021889897001593
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A new beamline for small-angle X-ray scattering (SAXS) has recently been constructed and is presently under final commissioning at the 2 GeV storage ring ELETTRA. It has been designed specifically for time-resolved studies of non-crystalline and fibrous materials and has been optimized for small-angle scattering measurements. The beamline operates with a SAXS resolution between 10 and about 1400 Angstrom in d spacing (at 8 keV) and has been optimized with respect to high flux at the sample [of the order of 10(13) photons s(-1) for 8 keV photons (2 GeV, 400 mA)]. Soon it will be possible to perform simultaneously wide-angle diffraction measurements in the d-spacing range 1.2-8 Angstrom (at 8 keV). In order to allow time-resolved (resolution similar to 1 ms) small-angle scattering measurements, a high-power 57-pole wiggler is used as the beamline source. From its beam, one of three discrete energies, 5.4, 8 and 16 keV, can be selected with a double-crystal monochromator, which contains three pairs of asymmetrically cut plane Si(111) crystals. Downstream, the beam is focused horizontally and vertically by a toroidal mirror. Commissioning tests of this new SAXS beamline showed that all design parameters have been realized.
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页码:872 / 876
页数:5
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