9-(4-Hydroxy-3-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,5,6-tetrahydro-9H-xanthene-1,8(2H,7H)-dione

被引:2
|
作者
Hasanudin, Noorhafizah [2 ]
Rahim, Aisyah Saad Abdul [2 ]
Mohamed, Nornisah [2 ]
Quah, Ching Kheng [1 ]
Fun, Hoong-Kun [1 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, Usm 11800, Penang, Malaysia
[2] Univ Sains Malaysia, Sch Pharmaceut Sci, Usm 11800, Penang, Malaysia
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2010年 / 66卷
关键词
X-RAY; DERIVATIVES;
D O I
10.1107/S1600536810020258
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
In the title compound, C24H28O5, the two cyclohexene rings adopt envelope conformations, and the planes through the coplanar atoms makes dihedral angles of 82.86 (6) and 77.90 (6)degrees with the benzene ring. The two cyclohexene rings make a dihedral angle of 5.33 (6)degrees between their least-squares planes. The pyran ring adopts a flattened boat conformation. In the crystal packing, molecules are linked into two-dimensional networks parallel to the ab plane via O-H center dot center dot center dot O and C-H center dot center dot center dot O interactions.
引用
收藏
页码:O1538 / U288
页数:13
相关论文
共 50 条
  • [31] Easy Access to 1H-Pyrrolo[3′,4′:5,6]pyrido[2,3-d]pyrimidine-2,4,6,8(3H,7H)-tetraone and Selectively N7-Substituted Analogues through Key Synthons
    Tourteau, Aurelien
    Merlet, Eric
    Bontemps, Alexis
    Leland, Mathilde
    Helissey, Philippe
    Giorgi-Renault, Sylviane
    Desbene-Finck, Stephanie
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2015, 2015 (32) : 7028 - 7035
  • [32] Crystal structure of (E)-7-hydroxy-2-((6-methoxypyridin-3-yl)methylene)-3, 4-dihydronaphthalen-1(2H)-one, C17H15NO3
    Zhang, Sheng-Nan
    Zhao, Feng-Lan
    Meng, Qing-Guo
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2022, 237 (01): : 1 - 3
  • [33] An efficient synthesis of (±) 4-hydroxy-9-methoxy-5,11-dimethy1-6H-1,2,3,4-tetrahydro-benzo[b]carbazolet
    Bengaouer, Mohamed Larbi
    Boukhari, Abbes
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2016, 55 (12): : 1532 - 1540
  • [34] The preparation of [closo-1-CB9H8-1-COOH-10-(4-C3H7C5H9S)] as intermediate to polar liquid crystals
    Pecyna, Jacek
    Denicola, Richard P.
    Ringstrand, Bryan
    Jankowiak, Aleksandra
    Kaszynski, Piotr
    POLYHEDRON, 2011, 30 (15) : 2505 - 2513
  • [35] Crystal structure of 6-hydroxy-5-((2-hydroxy-6-oxocyclohex-1-en-1-yl)(4-methoxyphenyl)methyl)-1,3-dimethylpyrimidine-2,4(1H,3H)-dione, C20H22N2O6
    Altowyan, Mezna Saleh
    Ali, M.
    Soliman, Saied M.
    Naser, Almoqbl A.
    Al-Majid, Abdullah Mohammed
    Barakat, Assem
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2018, 233 (04): : 747 - 749
  • [36] One-pot and solvent-free synthesis of 3-(9-hydroxy-3-methoxy-7-aryl-6,7,9,10-tetrahydro-5H-benzo [h]thiazolo [2,3-b] quinazolin-9-yl)-2H-chromen-2-ones and their antibacterial evaluation
    Velpula, Ravibabu
    Banothu, Janardhan
    Gali, Rajitha
    Sargam, Yakaiah
    Bavantula, Rajitha
    TURKISH JOURNAL OF CHEMISTRY, 2015, 39 (03) : 620 - 629
  • [37] 9-Furfurylidene-2,3-dimethyl-6,7,8,9-tetrahydro-4H-thieno[2′,3′:4,5]pyrimidino[1,2-a]pyridin-4one
    Bozorov, Khurshed A.
    Elmuradov, Burkhon Zh.
    Okmanov, Rasul Ya.
    Tashkhodjaev, Bakhodir
    Shakhidoyatov, Khusnutdin M.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O552 - U4450
  • [38] Convenient selective synthesis of 5,7,8,9-tetrahydro-4H,6H-chromeno[2,3-d][1,3]oxazin-4-ones
    Litvinov, Yu. M.
    Shestopalov, A. M.
    RUSSIAN CHEMICAL BULLETIN, 2009, 58 (02) : 479 - 481
  • [39] Synthesis, cytotoxicity, and antibacterial studies of 2,4,5,6-substituted hexahydro-1H-isoindole-1,3(2H)-dione
    Yetiskin, Egehan
    Gundogdu, Ozlem
    Mete, Derya
    Celebioglu, Neslihan
    Kara, Yunus
    Sanli-Mohamed, Gulsah
    CHEMICAL BIOLOGY & DRUG DESIGN, 2023, 102 (06) : 1448 - 1457
  • [40] Synthesis and crystal structure of di-tert-butyl 1"-acetyl-2,2",9′-trioxo-4a′,9a′-dihydro-1′H,3′H,9′H-dispiro[indoline-3,2′-xanthene-4′,3"-indoline]-1,3′-dicarboxylate, C39H38N2O9
    Li, Wu-Wu
    Liu, Xiong-Li
    Li, Xiao-Peng
    Zheng, Hao-Nan
    Weng, A-Tong
    Feng, Ling-Ying
    Liu, Lu
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2021, 236 (05): : 995 - 997