In situ synchrotron X-ray diffraction study of the effect of microstructure and boundary layer conditions on CO2 corrosion of pipeline steels

被引：48
|
作者：
Ko, M. [1 ,4 ]
Ingham, B. [2 ,5 ]
Laycock, N. [3 ]
Williams, D. E. [4 ,5 ]
机构：
[1] Quest Integr Grp, Lower Hutt 5045, New Zealand
[2] Callaghan Innovat, Lower Hutt 5010, New Zealand
[3] Univ Birmingham, Coll Engn & Phys Sci, Birmingham B15 2TT, W Midlands, England
[4] Univ Auckland, Sch Chem Sci, Auckland 1022, New Zealand
[5] Victoria Univ Wellington, Sch Chem & Phys Sci, MacDiarmid Inst Adv Mat & Nanotechnol, Wellington 6440, New Zealand
来源：
CORROSION SCIENCE | 2015年 / 90卷
关键词：
Low alloy steel; Carbon steel; X-ray diffraction; Potentiostatic; CARBON-DIOXIDE CORROSION; SCALE FORMATION; CHUKANOVITE; PRODUCTS; CHROMIUM; OIL;
D O I：
10.1016/j.corsci.2014.10.010
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
This study demonstrates that the nucleation of crystalline scales of siderite and chukanovite onto the surface of low-alloy steels under CO2 corrosion at elevated temperature is critically dependent on initial surface roughness, on microstructure-related surface roughness developed during corrosion, and on stirring in the solution. This study confirms that effects due to chromium micro-alloying in the steel are extremely important for siderite nucleation. On average, these effects dominate over the effects of microstructure. However, spatial variation of the corrosion deposit thickness indicates an interdependence between microstructure and chromium-enhanced siderite nucleation with the possibility of localised corrosion developing as a result. (C) 2014 Elsevier Ltd. All rights reserved.
引用
收藏
页码：192 / 201
页数：10
相关论文
共 50 条
  • [21] Microstructure evolution in copper under severe plastic deformation detected by in situ X-ray diffraction using monochromatic synchrotron light
    Kilmametov, A. R.
    Vaughan, G.
    Yavari, A. R.
    LeMoulec, A.
    Botta, W. J.
    Valiev, R. Z.
    MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2009, 503 (1-2): : 10 - 13
  • [22] Effect of H2S on the Corrosion Behavior of Pipeline Steels in Supercritical and Liquid CO2 Environments
    Choi, Yoon-Seok
    Hassani, Shokrollah
    Thanh Nam Vu
    Nesic, Srdjan
    Abas, Ahmad Zaki B.
    CORROSION, 2016, 72 (08) : 999 - 1009
  • [23] An in situ electrochemical impedance spectroscopy/synchrotron radiation grazing incidence X-ray diffraction study of the influence of acetate on the carbon dioxide corrosion of mild steel
    De Marco, Roland
    Jiang, Zhong-Tao
    John, Doug
    Sercombe, Matthew
    Kinsella, Brian
    ELECTROCHIMICA ACTA, 2007, 52 (11) : 3746 - 3750
  • [24] In situ synchrotron-based X-ray powder diffraction and micro-Raman study of biomass and residue model compounds at hydrothermal conditions
    Thomas, Morgan L.
    Butler, Ian S.
    Kozinski, Janusz A.
    ENERGY SCIENCE & ENGINEERING, 2015, 3 (03): : 189 - 195
  • [25] First stages of siderite crystallisation during CO2 corrosion of steel evaluated using in situ synchrotron small- and wide-angle X-ray scattering
    Ingham, Bridget
    Ko, Monika
    Laycock, Nick
    Kirby, Nigel M.
    Williams, David E.
    FARADAY DISCUSSIONS, 2015, 180 : 171 - 190
  • [26] In situ and operando x-ray diffraction and x-ray absorption studies of Co?TiO2 dry methane reforming catalysts
    Barrett, D. H.
    Forbes, R. P.
    Rodella, C. B.
    JOURNAL OF PHYSICS D-APPLIED PHYSICS, 2020, 53 (04)
  • [27] In situ high-pressure synchrotron X-ray diffraction study of the structural stability in the intermetallic compound Mn2Sb
    Yu, Z. H.
    Li, C. Y.
    Liu, H. Z.
    PHYSICA STATUS SOLIDI B-BASIC SOLID STATE PHYSICS, 2012, 249 (11): : 2239 - 2243
  • [28] Low temperature solid state synthesis of Li5FeO4 and CO2 capture mechanism via real time in situ synchrotron X-ray diffraction
    Blanco, Maria Valeria
    Kohopaa, Katja
    Snigireva, Irina
    Cova, Federico
    CHEMICAL ENGINEERING JOURNAL, 2018, 354 : 370 - 377
  • [29] Synchrotron radiation X-ray diffraction in situ study of fine-grained minerals in shock veins of Suizhou meteorite
    Xie, XD
    Shu, JF
    Chen, M
    SCIENCE IN CHINA SERIES D-EARTH SCIENCES, 2005, 48 (06): : 815 - 821
  • [30] First Seconds in a Building's LifeuIn Situ Synchrotron X-Ray Diffraction Study of Cement Hydration on the Millisecond Timescale
    Schlegel, Moritz-Caspar
    Sarfraz, Adnan
    Mueller, Urs
    Panne, Ulrich
    Emmerling, Franziska
    ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2012, 51 (20) : 4993 - 4996
12345